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第80楼2006/04/03
谢谢
celan 发表:下面列出150种基本的NMR实验名称,供有兴趣者参考.
(和200个NMR实验的资料见本主题帖后面的续贴)
150 Basic NMR Experiments
Chapter 1 The NMR Spectrometer
1.1 Principles of an NMR Spectrometer
1.1.1 The Magnet
1.1.2 The Spectrometer Console
1.1.3 The Workstation
1.1.4 Maintenance
1.2 Tuning a Probe-Head
1.2.1 Tuning and Matching with a Reflection Meter
1.2.2 Tuning and Matching with an R.F. Bridge and an Oscilloscope
1.2.3 Tuning and Matching with a Wobble Generator
1.3 The Lock Channel
1.4 The Art of Shimming
1.4.1 The Shim Gradients
1.4.2 The Shimming Procedure
1.4.3 Gradient Shimming
· Chapter 2 Determination of the Pulse-Duration
Exp. 2.1: Determination of the 90&; 1H Transmitter Pulse-Duration
Exp. 2.2: Determination of the 90&; 13C Transmitter Pulse-Duration
Exp. 2.3: Determination of the 90&; 1H Decoupler Pulse-Duration
Exp. 2.4: The 90&; 1H Pulse with Inverse Spectrometer Configuration
Exp. 2.5: The 90&; 13C Decoupler Pulse with Inverse Configuration
Exp. 2.6: Composite Pulses
Exp. 2.7: Radiation Damping
Exp. 2.8: Pulse and Receiver Phases
Exp. 2.9: Determination of Radio Frequency Power
· Chapter 3 Routine NMR Spectroscopy and Standard Tests
Exp. 3.1: The Standard 1H NMR Experiment
Exp. 3.2: The Standard 13C NMR Experiment
Exp. 3.3: The Application of Window Functions
Exp. 3.4: Computer-aided Spectral Analysis
Exp. 3.5: Line-Shape Test for 1H NMR Spectroscopy
Exp. 3.6: Resolution Test for 1H NMR Spectroscopy
Exp. 3.7: Sensitivity Test for 1H NMR Spectroscopy
Exp. 3.8: Line-Shape Test for 13C NMR Spectroscopy
Exp. 3.9 ASTM Sensitivity Test for 13C NMR Spectroscopy
Exp. 3.10: Sensitivity Test for 13C NMR Spectroscopy
Exp. 3.11: Quadrature Image Test
Exp. 3.12: Dynamic Range Test for Signal Amplitudes
Exp. 3.13: 13&; Phase Stability Test
· Chapter 4 Decoupling Techniques
Exp. 4.1: Decoupler Calibration for Homonuclear Decoupling
Exp. 4.2: Decoupler Calibration for Heteronuclear Decoupling
Exp. 4.3: Low Power Calibration for Heteronuclear Decoupling
Exp. 4.4: Homonuclear Decoupling
Exp. 4.5: Homonuclear Decoupling at Two Frequencies
Exp. 4.6: The Homonuclear SPT Experiment
Exp. 4.7: The Heteronuclear SPT Experiment
Exp. 4.8: 1D Nuclear Overhauser Difference Spectroscopy
Exp. 4.9: 1D NOE Spectroscopy with Multiple Selective Irradiation
Exp. 4.10: 1H Off-Resonance Decoupled 13C NMR Spectra
Exp. 4.11: The Gated 1H-Decoupling Technique
Exp. 4.12: The Inverse Gated 1H-Decoupling Technique
Exp. 4.13: 1H Single Frequency Decoupling of 13C NMR Spectra
Exp. 4.14: 1H Low-Power Decoupling of 13C NMR Spectra
Exp. 4.15: Measurement of the Heteronuclear Overhauser Effect
