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taoruo
第11楼2013/03/14
以下是checktune报告
Instrument Name Instrument 1 MS Model G6430A Tune Date & Time 2013-02-28 15:07 Data Path D:\MassHunter\Tune\QQQ\G6430A\Autotune_20130228_145821\atunes_20130228_150723_FAILED.TUNE.XML Ion Source ESI Ionization Mode ESI Positive Results Analyzer: MS1 Polarity: Positive Width: Unit X m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.3 118.1 0.1 -5.8 Adjust 11.0 0.7 0.1 10.3 Adjust 82029 #N/A #N/A 311.7 322.1 0.1 -10.4 Adjust 4.6 0.7 0.1 3.9 Adjust 64130 0 Pass 624.3 622.0 0.1 2.3 Adjust 25.0 0.7 0.1 24.3 Adjust 2863 0 Pass 922.0 922.0 0.1 0.0 Pass 25.0 0.7 0.1 24.3 Adjust 5967 0 Pass 1222.0 1222.0 0.1 0.0 Pass 25.0 0.7 0.1 24.3 Adjust 6025 0 Pass 1822.0 1822.0 0.1 0.0 Pass 25.0 0.7 0.1 24.3 Adjust 6009 0 Pass Analyzer: MS2 Polarity: Positive Width: Unit m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 118.1 118.1 0.1 0.0 Pass 0.7 0.7 0.1 0.0 Pass 26791 0 Pass 321.9 322.1 0.1 -0.2 Adjust 0.8 0.7 0.1 0.1 Pass 14192 0 Pass 621.9 622.0 0.1 -0.1 Pass 0.8 0.7 0.1 0.1 Pass 10793 0 Pass 921.9 922.0 0.1 -0.1 Pass 0.8 0.7 0.1 0.1 Pass 9605 0 Pass 1221.8 1222.0 0.1 -0.2 Adjust 0.8 0.7 0.1 0.1 Pass 12761 0 Pass 1821.7 1822.0 0.1 -0.3 Adjust 0.7 0.7 0.1 0.0 Pass 8561 0 Pass Analyzer: MS1 Polarity: Positive Width: Wide m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 117.9 118.1 0.3 -0.2 Pass 1.3 1.2 0.6 0.1 Pass 45543 0 Pass 321.8 322.1 0.3 -0.3 Pass 1.3 1.2 0.6 0.1 Pass 21964 0 Pass 622.1 622.0 0.3 0.1 Pass 25.0 1.2 0.6 23.8 Adjust 51 0 Pass 125.0 922.0 0.3 -797.0 Adjust 25.0 1.2 0.6 23.8 Adjust 35 0 Pass 125.0 1222.0 0.3 -1097.0 Adjust 25.0 1.2 0.6 23.8 Adjust 35 0 Pass 125.0 1822.0 0.3 -1697.0 Adjust 25.0 1.2 0.6 23.8 Adjust 0 0 Pass Analyzer: MS2 Polarity: Positive Width: Wide m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 118.1 118.1 0.3 0.0 Pass 1.2 1.2 0.6 0.0 Pass 35065 0 Pass 322.0 322.1 0.3 -0.1 Pass 1.3 1.2 0.6 0.1 Pass 20387 0 Pass 621.9 622.0 0.3 -0.1 Pass 1.3 1.2 0.6 0.1 Pass 15866 0 Pass 921.9 922.0 0.3 -0.1 Pass 1.3 1.2 0.6 0.1 Pass 18563 0 Pass 1221.8 1222.0 0.3 -0.2 Pass 1.3 1.2 0.6 0.1 Pass 29407 0 Pass 1821.8 1822.0 0.3 -0.2 Pass 1.2 1.2 0.6 0.0 Pass 31916 0 Pass Analyzer: MS1 Polarity: Positive Width: Widest m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 117.8 118.1 0.5 -0.3 Pass 2.6 2.5 1.3 0.1 Pass 60454 0 Pass 321.7 322.1 0.5 -0.4 Pass 2.7 2.5 1.3 0.2 Pass 34020 0 Pass 624.9 622.0 0.5 2.9 Adjust 1.2 2.5 1.3 -1.3 Pass 459 0 Pass 125.0 922.0 0.5 -797.0 Adjust 25.0 2.5 1.3 22.5 Adjust 35 0 Pass 125.0 1222.0 0.5 -1097.0 Adjust 25.0 2.5 1.3 22.5 Adjust 35 0 Pass 1821.9 1822.0 0.5 -0.1 Pass 25.0 2.5 1.3 22.5 Adjust 35 0 Pass Analyzer: MS2 Polarity: Positive Width: Widest m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 118.0 118.1 0.5 -0.1 Pass 2.6 2.5 1.3 0.1 Pass 57077 0 Pass 322.0 322.1 0.5 -0.1 Pass 2.6 2.5 1.3 0.1 Pass 36102 0 Pass 621.9 622.0 0.5 -0.1 Pass 2.8 2.5 1.3 0.3 Pass 25740 0 Pass 922.0 922.0 0.5 0.0 Pass 2.5 2.5 1.3 0.0 Pass 31926 0 Pass 1222.0 1222.0 0.5 0.0 Pass 2.4 2.5 1.3 -0.1 Pass 52272 0 Pass 1821.9 1822.0 0.5 -0.1 Pass 2.5 2.5 1.3 0.0 Pass 61962 0 Pass ¹ NOTE: 1) Actual abundances depend on many factors and are instrument specific. To change the minimum abundance, edit the values on the "Options" sheet. Negative Results Analyzer: MS1 Polarity: Negative Width: Unit X m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.9 113.0 0.1 -0.1 Pass 0.8 0.7 0.1 0.1 Pass 26310 0 Pass 301.9 302.0 0.1 -0.1 Pass 0.7 0.7 0.1 0.0 Pass 118681 0 Pass 607.6 602.0 0.1 5.6 Adjust 10.5 0.7 0.1 9.8 Adjust 15897 0 Pass 607.6 1034.0 0.1 -426.4 Adjust 10.5 0.7 0.1 9.8 Adjust 0 0 Pass 607.6 1334.0 0.1 -726.4 Adjust 10.5 0.7 0.1 9.8 Adjust 0 0 Pass 607.6 1933.9 0.1 -1326.3 Adjust 10.5 0.7 0.1 9.8 Adjust 0 0 Pass Analyzer: MS2 Polarity: Negative Width: Unit m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.9 113.0 0.1 -0.1 Pass 0.7 0.7 0.1 0.0 Pass 292437 0 Pass 301.9 302.0 0.1 -0.1 Pass 0.7 0.7 0.1 0.0 Pass 128332 0 Pass 601.9 602.0 0.1 -0.1 Pass 0.7 0.7 0.1 0.0 Pass 416108 0 Pass 1033.8 1034.0 0.1 -0.2 Adjust 0.7 0.7 0.1 0.0 Pass 576498 0 Pass 1333.8 1334.0 0.1 -0.2 Adjust 0.7 0.7 0.1 0.0 Pass 962218 0 Pass 1933.7 1933.9 0.1 -0.2 Adjust 0.8 0.7 0.1 0.1 Pass 638405 0 Pass Analyzer: MS1 Polarity: Negative Width: Wide m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.9 113.0 0.3 -0.1 Pass 1.2 1.2 0.6 0.0 Pass 32043 0 Pass 301.8 302.0 0.3 -0.2 Pass 1.3 1.2 0.6 0.1 Pass 175388 0 Pass 607.4 602.0 0.3 5.4 Adjust 10.7 1.2 0.6 9.5 Adjust 17282 0 Pass 125.0 1034.0 0.3 -909.0 Adjust 25.0 1.2 0.6 23.8 Adjust 36 0 Pass 1334.0 1334.0 0.3 0.0 Pass 25.0 1.2 0.6 23.8 Adjust 39 0 Pass 1933.9 1933.9 0.3 0.0 Pass 25.0 1.2 0.6 23.8 Adjust 40 0 Pass Analyzer: MS2 Polarity: Negative Width: Wide m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 113.0 113.0 0.3 0.0 Pass 1.2 1.2 0.6 0.0 Pass 387095 0 Pass 301.9 302.0 0.3 -0.1 Pass 1.2 1.2 0.6 0.0 Pass 189791 0 Pass 601.8 602.0 0.3 -0.2 Pass 1.3 1.2 0.6 0.1 Pass 744957 0 Pass 1033.8 1034.0 0.3 -0.2 Pass 1.3 1.2 0.6 0.1 Pass 1392607 0 Pass 1333.7 1334.0 0.3 -0.3 Pass 1.2 1.2 0.6 0.0 Pass 2866173 0 Pass 1933.6 1933.9 0.3 -0.3 Pass 1.2 1.2 0.6 0.0 Pass 2206217 0 Pass Analyzer: MS1 Polarity: Negative Width: Widest m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.8 113.0 0.5 -0.2 Pass 2.7 2.5 1.3 0.2 Pass 39615 0 Pass 301.8 302.0 0.5 -0.2 Pass 2.8 2.5 1.3 0.3 Pass 257529 0 Pass 604.8 602.0 0.5 2.8 Adjust 1.4 2.5 1.3 -1.1 Pass 60341 0 Pass 125.0 1034.0 0.5 -909.0 Adjust 25.0 2.5 1.3 22.5 Adjust 36 0 Pass 125.0 1334.0 0.5 -1209.0 Adjust 25.0 2.5 1.3 22.5 Adjust 0 0 Pass 125.0 1933.9 0.5 -1808.9 Adjust 25.0 2.5 1.3 22.5 Adjust 0 0 Pass Analyzer: MS2 Polarity: Negative Width: Widest m/z m/z Exp Tolerance Delta Result FWHM FWHM Exp Tolerance Delta Result Abundance Minimum1 Result 112.9 113.0 0.5 -0.1 Pass 2.6 2.5 1.3 0.1 Pass 536778 0 Pass 301.9 302.0 0.5 -0.1 Pass 2.6 2.5 1.3 0.1 Pass 287462 0 Pass 601.9 602.0 0.5 -0.1 Pass 2.6 2.5 1.3 0.1 Pass 1114457 0 Pass 1033.9 1034.0 0.5 -0.1 Pass 2.5 2.5 1.3 0.0 Pass 2457502 0 Pass 1333.8 1334.0 0.5 -0.2 Pass 2.5 2.5 1.3 0.0 Pass 5538127 0 Pass 1933.8 1933.9 0.5 -0.1 Pass 2.3 2.5 1.3 -0.2 Pass 5264742 0 Pass ¹ NOTE: 1) Actual abundances depend on many factors and are instrument specific. To change the minimum abundance, edit the values on the "Options" sheet. sukiliang(sukiliang) 发表:http://bbs.instrument.com.cn/shtml/20130217/4570465/index_2.shtml
有这个这么差么？