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  • myreebok

    第31楼2007/04/23

    实在是连复制粘帖的兴趣也没有,直接看不就得了,如果楼主有中文需要,直接说就得了,觉得太做作了

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  • zhongnuo

    第32楼2007/04/24

    有翻译好的吗?

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  • 茅茅

    第33楼2007/04/24

    有两名新手都帖出了翻译好的文字,都很不错。等五一期间我再结帖,顺便点评。

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  • Easy-Boy

    第34楼2007/04/25

    Apparatus— A liquid chromatograph consists of a reservoir(原义是水库) containing the mobile phase, a pump to force the mobile phase through the system at high pressure, an injector to introduce the sample into the mobile phase, a chromatographic column, a detector, and a data collection device such as a computer, integrator, or recorder. Short, small-bore columns containing densely packed particles of stationary phase provide for the rapid exchange of compounds between the mobile and stationary phases. In addition to receiving and reporting detector output, computers are used to control chromatographic settings and operations, thus providing for long periods of unattended operation.

    仪器--液相色谱由流动相储液系统、给流动相提供高压的泵系统、将样品引入流动相的进样器、色谱柱、检测器和数据采集设备,如一个计算机、积分器、或记录仪。装填有固定相填料的细颈色谱柱使化合物在流动相和固定相中快速交换中得以分离,然后通过检测器检测和输出报告,计算机一般用来控制色谱仪设置和操作,并在无人操作时提供自动运行。

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  • Easy-Boy

    第35楼2007/04/25

    Pumping Systems—HPLC pumping systems deliver metered amounts of mobile phase from the solvent reservoirs to the column through high-pressure tubing and fittings. Modern systems consist of one or more computer-controlled metering pumps that can be programmed to vary the ratio of mobile phase components, as is required for gradient chromatography, or to mix isocratic mobile phases (i.e., mobile phases having a fixed ratio of solvents). However, the proportion of ingredients in premixed isocratic mobile phases can be more accurately controlled than in those delivered by most pumping systems. Operating pressures up to 5000 psi or higher, with delivery rates up to about 10 mL per minute are typical. Pumps used for quantitative analysis should be constructed of materials inert to corrosive mobile phase components and be capable of delivering the mobile phase at a constant rate with minimal fluctuations over extended periods of time.
    泵系统—HPLC 泵系统通过高压管路和设备将储液系统的流动相按设定的流量精确地输送通过柱子,最新的泵系统由一台或更多的计算机测量控制泵使得流动相组分能够按照程序变化改变比例,如有必要,可以进行梯度洗脱或混合均匀的流动相(i.e.,流动相可以是混合比例的溶液),然而,当操作压力达到或高于5000 psi,流速达到10ml/min的典型值时,预混合均匀的流动相各成分的比例就比泵控制的更精确。泵系统在定量分析中要能够耐腐蚀性流动相物质,并在较长的时间内保持一个恒定的流速和极小的波动。

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