redanqi 发表:提取
称取20.0g经粉碎并过20目筛的大米样品置具塞锥形瓶中,加入50mL丙酮,于电动振荡器上振荡30min,用快速定性滤纸过滤于烧杯中,残渣再用30mL丙酮按上法再提取一次。用30mL丙酮分次洗涤残渣,洗液并入烧杯中,于水浴(50℃)上挥发浓缩近干。
3.1 Extraction
Weigh 20g of rice sample grinded and passed the 20 mesh sieve to a flask with stopper, add 50 ml of acetone, shake for 30 minutes by the electrodynamic shaker, filter to a beaker through quick qualitative filter paper, extract the residue once more using the above method by 30 ml of acetone. Wash the residue by 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dry on the water bath of 50℃.
3.1 Extraction
Weigh 20.0g of ground rice sample that passes 20 mesh to a conical flask with stopper. Add 50 ml of acetone and shake for 30 minutes with electric shaker(agitator). The mixture is then filtered to a beaker through quick qualitative filter paper, and the residue will be extracted once more using the above mentioned method through 30 ml of acetone. Wash the residue through (by) 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dryness in the water bath at 50℃.