ChromaTOF软件系统基础培训教程

目录 一、ChromaTOF.软件概述 ...................................................................................................... 3 1. 软件登录 .......................................................................................................................... 3 2. 软件界面浏览 .................................................................................................................. 4 2.1 工作区 ........................................................................................................................ 5 2.2 工具栏 ........................................................................................................................ 5 2.3 状态栏 ........................................................................................................................ 9 2.4标题栏按钮列表 ....................................................................................................... 10 3.管理数据库 ...................................................................................................................... 15 3.1创建数据库连接 ....................................................................................................... 15 3.2选择数据库连接 ....................................................................................................... 19 3.3选择默认数据库连接 ............................................................................................... 20 3.4删除数据库连接 ....................................................................................................... 20 4. 创建方法 ........................................................................................................................ 21 4.1 创建自动进样方法 .................................................................................................. 21 4.2 创建气相色谱方法 .................................................................................................. 24 4.3 创建质谱方法 .......................................................................................................... 27 4.4 创建数据处理方法 .................................................................................................. 28 4.5 创建QC方法 ........................................................................................................... 34 4.6 创建调谐方法（Tune Methods） .......................................................................... 37 5. 仪器日常优化（ Daily Instrument Check） ................................................................ 37 6. 样品采集流程 ................................................................................................................ 38 7. 数据处理流程 ................................................................................................................ 39 8.定性分析流程 .................................................................................................................. 40 9.定量校正流程 .................................................................................................................. 41 10.峰表 ............................................................................................................................... 42 11.色谱图 ............................................................................................................................ 46 12.3D图浏览程序 .............................................................................................................. 51 13.质谱图 ............................................................................................................................ 54 14.样品对比分析（Reference Procedures） .................................................................... 56 2 15.保留指数（Retention Index Procedures） ................................................................... 57 16.分类（Classifications） ................................................................................................. 57 17.自建谱库（Create User Library） ................................................................................. 59 18.用户报告（Customize Reports） .................................................................................. 59 19.文件导入导出（Import and Export Files） .................................................................. 62 20.数据备份和读取（Backup to Archive and Restore from Archive）............................. 63 二、仪器常规操作和维护 ..................................................................................................... 64 1. 仪器工作条件 ................................................................................................................ 64 2. 开机程序 ........................................................................................................................ 64 3. 关机程序 ........................................................................................................................ 64 4. 更换色谱柱 .................................................................................................................... 65 5. 充液氮 ............................................................................................................................ 65 6. 清洗机箱过滤网 ......................................................................................................... 66 7. 机械泵的维护 ............................................................................................................. 66 8. 色谱系统的维护 ......................................................................................................... 66 9. 质谱系统的维护 ......................................................................................................... 67 10．系统检漏和维护 ............................................................................................................. 67