祥鹄微波超声波紫外光组合仪合成二甲硫醚锂

二甲硫醚锂是许多药物合成的重要中间体，其合成受到越来越多的关注。本实验旨在利用微波、超声波及紫外组合催化方法合成硫醚锂，并与常规方法进行比较。结果发现组合催化方法在合成过程的具有较大优势，可缩短反应时间，而且在同样的反应时间下提高产率，具有较大的研究价值及广泛的应用价值。 Dimethyl sulfide lithium is an important intermediate compound of drug synthesis, and is causing more and more attention. This study was designed to use the microwave, ultrasound and UV combination method to catalytic synthesis of dimethyl sulfide lithium, and compared with the conventional method. The results showed that the combination of catalytic methods have greater advantages in the synthesis process, shorten the reaction time and enhance product yield under the same reaction time.It has greater research value and extensive practical value.