Microwave-Assisted One-Pot Synthesis of 1-Indanones from Arenes and α β-Unsaturated Acyl Chlorides

2007/03/22   下载量: 324

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参考标准 论文发表在“The Journal of Organic Chemistry”

o-Dichlorobenzene was dried over anhydrous sodium sulfate and distilled prior to use.All reactions were performed in a commercial microwave reactor(XH-100A,100-1000W,Beijing Xianghu Science and Technology Development Co.Ltd,Beijing,P.R.China).The temperature of the reaction mixture was measured by an immersed platinum resistance thermometer.Melting points were measured on a melting point apparatus and are uncorrected.H NMR(200 or 300 MHz)and C NMR(50 or75MHz)spectra were obtained on an EI mass spectrometer.IR spectra were recorded on a FT-IR spectrometer with an OMNI sampler.TLC separations were performed on silica gel GF plates ,and the plates were visualized with UV light.

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