色谱脱气方法

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色谱脱气方法相关的厂商

  • 深圳通瑞色谱仪器有限公司是一家专业从事液相色谱仪研发、设计、生产与销售的高科技企业, 开发了具有先进水平的GI-3000液相色谱系统、GI-3000XY血药浓度分析仪、GI-5200多功能离子色谱仪系统,产品已在医疗、食品、制药、环境环保、科研、高校科研实训、生物、石油化工等多行业领域使用。通瑞仪器注重于技术创新,紧盯国际新技术,推出了高性能双直线电机驱动精密滚珠丝杆的恒流泵输液系统(第三代技术,与waters,2695、安捷伦1260方案相同),达到国际先进技术水平。目前研发完成GI-3000XY血药浓度分析仪(全智能二维液相色谱系统),系统集成了,医院多科室上百种药物成分及其浓度的测定方法,为儿童的健康成长发育以及需要长期治疗、精准治疗的大病与慢性病患者,制定精准医疗方案,提供了科学支持,本系统也适用于常见药物的临床药物分析研究。 公司主要产品:GI-3000高效液相色谱仪系列产品,研发完成四元低压梯度液相色谱仪,目前是国率先家采用直线电机驱动滚珠丝杆的恒流泵输液系统(同waters2695方案),技术先进,具有完全自主知识产权。
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  • 南京仁华色谱科技应用开发中心是专业从事色谱仪器技术和应用研究开发、生产经营和服务的高科技企业,同时代理和配套国内外先进分析仪器。公司致力于气相色谱分析方案整体解决的研究,为客户从售前仪器选型咨询、分析方法开发、仪器安装调试、使用人员技术培训、售后技术支持等全方位提供交钥匙式一揽子价廉质优的服务,让客户真正“买得放心,用得安心”,彻底免除仪器使用的后顾之忧。  公司自2004年成立以来业绩不断扩大,成功完成了多项色谱分析方案的开发与应用:油品及馏份油模拟蒸馏气相色谱分析系统,燃气(包括天然气、液化石油气、人工煤气、合成燃气等)专用气相色谱分析及热值测定系统,炼厂气专用气相色谱分析系统,煤制甲醇催化制轻烃汽油气相色谱分析系统,大气中痕量笑气N2O专用气相色谱分析系统,大气中非甲烷总烃和苯系物分析系统,汽油中甲乙醇含量气相色谱分析系统,高纯氢微量杂质和纯度色谱分析系统,食品级二氧化碳中微量苯及其他芳烃含量气相色谱分析系统,有机化工产品中微量水份含量专用气相色谱分析系统(带反吹功能),工业级六氟化硫SF6过程控制及产品质量分析专用气相色谱系统,电子级八氟丙烷CF8过程控制及产品质量分析专用气相色谱系统,精丙烯、精乙烯全分析气相色谱系统,二甲醚气相色谱分析系统,沼气气体成份及沼液中有机酸气相色谱分析系统,矿井气气相色谱分析系统,加氢脱硫催化剂性能评价气相色谱分析系统,储油罐中油气含量在线分析气相色谱系统、秸秆等生物质高温汽化气体成份在线气相色谱分析系统等等。  多年来,公司成功运用国内技术领先的GC9890系列气相色谱仪为许多客户单位解决了各种应用分析课题,得到了广大在用客户的好评。目前公司与中国石油大学、东南大学、南京中医药大学、南京农业大学、南京林业大学、西南石油大学、中国矿业大学、南京工业大学、中科院南京土壤研究所、江苏省农业科学研究院、安徽省产品质量监督检验研究院等科研院所均有良好的合作,从而赢得了高等院校、质检、科研机构、特种气体、环保、石化、化工、化肥、煤矿、制药、食品、电力、酿酒等众多领域客户的青睐。 由于GC9890B/A气相色谱仪等效采用了安捷伦公司5890气相色谱仪核心技术,许多用过安捷伦公司气相色谱仪的用户使用我公司产品也觉驾轻就熟,所以客户逐年增多。  公司拥有一支经验丰富、素质过硬的技术队伍,不乏具有长年在仪器生产、分析应用方面的高级工程师和专业技术人员,为客户仪器的顺利使用提供了强有力的技术保障。“诚信、守诺、服务社会”是我们的信念,“质量第一、信誉第一、真诚服务求发展”是我们的宗旨;为您服务,我们以此为荣;您的满意是我们不懈的追求,热忱欢迎您的惠顾。
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  • 400-860-5168转4265
    “苏州汇通色谱分离纯化有限公司”是一家以自主知识产权技术和产品为核心,具有独立研发能力的高技术企业,主要以药厂、生物制品企业、高纯度化学制品企业、质量鉴定单位、大学、科学研究机构和生物技术公司为目标客户,提供高效、高选择性制备色谱分离柱产品;高纯度产品色谱纯化工程设计以及高纯度产品纯化服务。与市场上现存公司相比,本公司拥有高科技(特殊设计)的专利分离介质,高纯度色谱纯化工程设计核心能力,已发展高通量、高选择性、高分离效率的模块式分离系列产品及配套的相应方法;公司除为企业提供高性能的色谱分离柱系统系列产品外,还可以直接为企业提供复杂样品体系的纯品,为企业“工程化”提供一条龙服务;既结合色谱分离专家的理论与实践,为客户发展复杂样品体系的分离、分析、纯化制备方法和有效的工具,同时为市场提供色谱纯度的试剂级产品。
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色谱脱气方法相关的仪器

  • HTY-DG131 脱气仪 400-860-5168转1222
    概述HTY-DG131型真空脱气仪是我公司独立研发的专门用于纯化水、蒸馏水和去离子脱气的设备,可快速而安全的去除水中溶解的气体。完全符合《中国药典》(2010版)的规定,可代替人工煮沸法和其他的脱气方法,省时、省力,提高工作效率。 应用领域药物研究、制药、化工等行业 工作原理利用脱气膜的扩散原理将水中的气体去除,同时溶液在进入脱气膜前进行加热,使气体在水中的溶解度降低,提高脱气效率。产品特点从启动到可使用不到5分钟(一般为3分钟),大大缩短了准备时间,随时都可操作运行,提高工作效率。无溶液体积上限,只要水源充足,就可持续脱气供水。一键实现进液、加热、脱气功能。采用大屏幕液晶显示屏,中文菜单提示,仪器操作简便。具有故障自诊功能,出现异常情况时,设备自动停止运行并出错提醒。具有断电保护功能,功率过大时,会自动断电,减少设备的损伤。具有记忆存储功能,可保存客户上一次的设置参数。具有温度补偿和校准功能。技术参数温度控制范围:37.0℃~42.0℃分辨率:0.1℃控温精度:± 0.5℃脱气真空度:0.08~0.09 Mpa分辨率:0.01 Mpa处理容积体积:无上限,视入水口水量而定。脱气后溶氧量:&le 2.8mg/L最大功率:2500W电 源:220V ± 10%,50 ± 1Hz
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  • 仪器简介:FloVac 脱气站将两种不同的样品准备技术融合一体,自由选择。这个单机设备具有6个脱气端口,各站具有独立控制阀门,可以在不中断其它样品的情况下加载或卸载某个样品管。 一个内置加热包提供用户可选的脱气温度至400°C,步进10°C。数字显示,连续检测温度。FloVac 脱气站可以满足NOVA,QUADRASORB™ SI或AUTOSORB-1 系列比表面和孔径分析仪的连续样品准备的需要。 Flow 脱气站仅用于实验室流动脱气的需要。 主要特点:- FloVac 脱气站将两种不同的样品准备技术融合一体,自由选择。- 具有6个脱气端口,各站具有独立控制阀门,可以在不中断其它样品的情况下加载或卸载某个样品管。 - 一个内置加热包提供用户可选的脱气温度至400°C,步进10°C。- 数字显示,连续检测温度。FloVac 脱气站可以满足NOVA,QUADRASORB™ SI或AUTOSORB-1 系列比表面和孔径分析仪的连续样品准备的需要。 当作为流动脱气站使用时,应仔细调节针阀,控制气流速度,以避免超细粉样品的扬析(吹出)。各站均配有金属吹扫管,它可以调节插入样品管的深度,适合所有样品管。样品脱气后,可将样品管放入对应的冷却站内。 当作为真空脱气站使用时,可选择抽空速率和回填气。附件包括适用于三种不同管颈及长度的样品管接口配件。
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  • 仪器简介:MasterPrep 脱气站为6 站真空和流动脱气站,配合AUTOSORB, QUADRASORB™ SI 以及NOVA 系列比表面和孔径分析仪进行大批量样品准备。 6 个脱气端口各自具有独立的加热炉,独立的数字温度控制,独立的冷却站,允许多种样品在不同条件下同时准备。 可用流动脱气和真空脱气两种方式操作。对任何类型的材料都可找到可行的样品准备方法。 流动速率和真空脱气速率可调。 六通道数字温度控制器使每个样品脱气端口各自具有独立的程序升温功能(多达20步)。 升温程序可连接计算机进行控制,也可在控制器上直接进行设置。 6个独立的冷却站在流动脱气或真空脱气后将样品冷却至室温。 技术参数:温度: 六通道数字温度控制器 双路升温程序: 可从计算机软件中进行选择,也可在控制器上直接进行设置 用户可分别设定温度爬升速率和保持时间(各站最多20段) 四位温度显示 口令保护功能 温度设定:1º C 递进 准确度(样品处):+/- 5 º C 或设定点的 +/-5% 环境: 周围温度:15 to 40º C 最大相对湿度:80% 无冷凝安全性: 符合CE标准 各站均有独立断热开关,以防过热 内置冷却风扇 电源: 电压:100 - 240 VAC, 50/60Hz 功率:600 VA(不包括真空泵)体积: 高 28.6 cm, 长64.8 cm, 宽43.2 cm重量: 20.7 kg运行要求: 纯度99.99%的干燥氮气或氦气,精确调节输出压力至7 psia 真空泵:至少能达到20 millitorr 的真空度 主要特点:性能: 具有六个样品准备站(端口) 温度范围:室温至425º C 流动脱气方式或真空脱气方式 各站独立温度控制 用户可选回填气/吹扫气(常用 N2 或 He) 当达到用户指定的真空度时,自动触发并转换阀门由慢(精细)抽真空到快(粗放)抽真空,以防止粉末样品扬析 在流动脱气方式下,各站流动速率可独立调节,高至100 ml / min 六个独立的冷却站 适用于6,9和12mm颈杆外径的样品管 数字真空圭表显示真空度
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色谱脱气方法相关的资讯

  • 高效液相色谱日常维护要点-脱气
    大家好,高效液相色谱和其它常规分析仪器一样,为了能让高效液相色谱更好的工作、在实验的时候得到可靠的数据,首先你要保养好它,使它处于一个健康的待机状态,这样你使用它进行检测分析时就可以比较顺利地获得理想结果。而且良好规范的操作习惯还可以延长仪器使用寿命。在日常使用维护中最重要的主要有三点:脱气、过滤和冲洗。这三点属于最常规操作要求,同时也是检测分析中必不可少的流程。小编会分三期为大家讲解,今天先带大家了解下脱气的具体原因和脱气的具体方法。脱气流动相里存在气泡是HPLC系统操作过程中常见的问题、气泡会造成泵输出的问题,也能造成检测器的输出结果中出现假的色谐峰。大多数的气泡问题可以在使用流动相之前以脱气的方法来消除。下面就是小编简单总结了脱气的主要目的:1、防止由溶解(在液体中的)气体量的变动引起的检测不稳程度 。2、提高保留时间和色谱峰面积的重现性。3、防止气泡引起尖峰。4、使基线稳定,提高信噪比。5、防止由气泡的产生引起的故障,示差折射率检测器:使折射率变化UV检测器(200nm以下):溶解氧气有吸收,荧光检测器:溶解氧气有消光作用。6、减少死体积。7、防止填料氧化。脱气要求只要空气在流动相里保持溶解,气泡问题就很少会出现。原则上讲人工配备的等度洗脱流动相般不需要脱气就可以在实验中使用,但是被气体饱和的溶液也只需要非常小的压力下降就能脱气。比如当流动相通过溶剂人口的在线过滤器,或者当流动相进人压力相对低的检测器溶液池时。因为这个原因和为了能使一般的HPLC操作具有可靠性,我们强烈建议用于反相色谱的所有溶剂都必须经过脱气。脱气对于正相HPLC来说不会产生很多问题,所以使用正相色谱时脱气是可选的。需要除去的溶解在流动相里的气体量根据HPLC泵的设计不同而不同,一些泵能够承受大量溶解在流动相里的气体而另外些泵则需要彻底脱气才能达到可靠的操作效果。常用的脱气方法1.抽真空脱气法:此法可使用真空泵,降压至0.05~0.07MPa即可除去溶解的气体,用真空脱气10-15分钟可以除去60%-70%溶解在流动相的气体。但是由于真空脱气会使混合溶剂组成发生变化,从而影响到实验的重现性,因此多用于单溶剂体系的简单分析。2.氦气喷洗脱气法:氦气喷洗是除去流动相里的气体最有效的技术,主要是利用氦气在液体中溶解度比空气低的特性,在0.1MPa压力下,以约60mL/min流速通入流动相储液容器中10~15min,可以很有效地从流动相中排除溶解的空气,能排除接近80%-90%溶解的气体。采用一个高效分布式喷射流装置,一体积的氦气可从流动相中将等体积的几乎全部气体排除。3.在线脱气法:在线脱气主要优点是操作简单,低故障,并非常有效。4.加热回流法:此法的脱气效果较好。但是还是有一些不足,那就是在操作时要特别注意冷凝塔的冷却效率,否则溶剂会丢失,混合流动相的比例会有变化。5.超声波脱气法:实验室最普遍的脱气方法,主要操作就是将欲脱气的流动相置于超声波清洗器中,用超声波震荡时间不宜过长,避免温度升高导致易挥发性成分的丢失,一般在5min之内。但是相对于其他脱气方法,优点是容易操作,时间短。不足之处则是此法的脱气效果相对较差。到此需要脱气的具体原因和脱气的具体方法,在这里就差不多介绍完了。下期小编将继续带领大家去具体了解高效液相色谱日常维护要点-过滤。
  • 您目前使用的脱气技术是否限制了液相色谱分析的进步?
    您目前使用的脱气技术是否限制了液相色谱分析的进步?您目前使用的脱气技术是否限制了液相色谱分析的进步?★PROBLEMHave your current degassingmethods reached the limit foradvancing your liquidchormatography analyses?高效液相色谱法的关键在于结果一致性。因此,当流动相气体析出时,使用适合流路的在线脱气技术,对于稳定系统流速并提高色谱准确度至关重要。然而,需要考虑因素有很多… … 艺达思提供优质的液相色谱分析脱气技术您可以点击https://www.instrument.com.cn/netshow/SH101586/ ,获取相关产品信息。或者给我们 400-860-5168转1586 留言,了解更多最新的技术。请关注艺达思微信公众号,微信搜索“艺达思健康与科学,查看相关视频”
  • 发布:液相色谱脱气创新技术
    h2 class=" rich_media_title" id=" activity-name" style=" margin: 0px 0px 14px padding: 0px color: rgb(51, 51, 51) text-transform: none line-height: 1.4 text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " 发布:液相色谱脱气创新技术 /h2 p strong span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 新一代技术让 /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 24px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " HPLC /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 脱气可控 /span /strong /p section style=" margin: 0px 8px 0.1px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none line-height: 25.5px text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px font-size: 12px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 18px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " Carl Sims, span class=" Apple-converted-space" & nbsp /span /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 18px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 首席科学家 /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 18px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " , IDEX Health & amp Science /span /span /section p br/ /p section style=" margin: 0px 8px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 12.84px font-family: Arial, sans-serif font-size: 12px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 600 Park Court, RohnertPark, CA 94928 csims@idexcorp.com /span /section p br/ /p p br/ /p p & nbsp /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 近年来,围绕着分析领域的技术和仪器优化的基本研究之外,分析实验的每个领域都需要采用现代管理和生产流程。基于 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " QbD /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " (质量源于设计)理念的方法越来越多,并且需要进行主动生命周期管理;实验室中的大多数仪器 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " - /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 例如从高端液质联用( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC-MS /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )系统到较简单的离心机、天平和泵,都集成至控制软件和实验室管理工具中。目标都集中在:可重复 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " / /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 可验证的性能,效率最大化,经济的运营方式,以及越来越被重视的环保意识。 /span /p p span style=" text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 这种变化的结果是,随着分析仪和实验室设备的更新,可以引入支持这一转变的分析领域的技术创新的新模型。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 在本文中,我们将研究 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 装置的重要组成部分,即脱气机,该装置迄今仍未满足当今的趋势。我们呈上多年开发过程的研究成果,以重新评估此关键部件的设计,性能和可控性,并重点介绍新型通用型平面薄膜脱气机的数据。 /span /p p style=" text-align: center " img title=" 5.jpg" style=" max-height: 100% max-width: 100% " alt=" 5.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/73ac5970-516d-4d88-8afe-ffe120d9043e.jpg" / /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 这项新技术通过允许用户为任何 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统或方法选择和控制固定的脱气效率,从而将重点从“恒定真空”转移到“恒定性能”。 /span /p p span style=" margin: 0px padding: 0px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 脱气技术的背景 /span /strong /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 减少 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 流动相中的溶解空气量会对系统流速和流动相组成的稳定性产生重大影响。低压混合 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 泵仅依靠溶剂进入泵,在从比例阀转移到入口单向阀的过程中,发生的任何气体析出都会导致多种类型的错误。首先,会发生组分错误,因为传输线中的体积包含了空气,并不完全是流动相。随着传输线中气泡的伸展扩张,混合物的精度会继续下降。最后,进入泵的气泡可能会干扰入口单向阀,从而使泵无法将全部体积的流动相输送到色谱柱,而是将一部分移回比例阀。此外,在将流动相输送到色谱柱之前,泵也会将所有气泡压缩到系统压力。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 在高压混合 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统中,溶解的气体会影响入口单向阀的操作,它会由于气蚀而形成微气泡。与低压混合 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 泵一样,气泡会导致流量不正确,从而影响保留时间。根据检测器的类型和对流量的敏感性,这种波动的流量还会增加检测器中的系统噪音。因此,溶解的空气影响分离的准确性和分离度,以及可靠地鉴定色谱柱上已分离化合物的能力。所以,长期以来,基本上所有的 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统都包括某种形式的脱气,从真空脱气,氦气鼓泡,超声处理到采用膜技术(包括 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " PTFE /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 膜和 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " Teflon /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " & #8482 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " AF /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )的在线方法。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 当今的 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统具有两种流动相混合装置之一:要么在溶剂进入泵之前就对其进行混合(低压混合);或者,流动相混合发生在泵之后但进样阀之前(高压混合)。在这两种情况下,对流动相混合物及其组分进行有效的在线真空脱气有助于避免色谱问题。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 1975 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 年, /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " Tokunaga /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 发表了数据集,该数据集为 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 溶剂混合物的脱气奠定了基础 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " [1] /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 。他确定了氧气在各种醇 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " - /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 水混合物中的溶解度的奥斯特瓦尔德系数,并演示了为防止气泡形成混合物需要脱气的程度。这篇开创性的论文为当今大多数实验室日常使用的基于 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 管式 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 的脱气系统的开发奠定了基础。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 1 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 绘制了 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " Tokunaga /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 的数据,并以 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统将流动相混合为体积百分比的方式重新计算。上方的实心红色线和奥斯特瓦尔德系数的线之间的差值的代表混合物中溶解的空气过饱和度。还展示了通过脱气减少空气量的三条示例曲线。 /span /p p style=" text-align: center " img title=" 6.jpg" style=" max-height: 100% max-width: 100% " alt=" 6.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/6fda221f-2d60-4f6e-a805-f0ce99dd64f7.jpg" / /p p & nbsp /p p span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " em 图 /em /span em style=" margin: 0px padding: 0px text-align: justify color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 1. Tokunaga 1975 /span /em em style=" margin: 0px padding: 0px text-align: justify color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 年论文的数据,以体积%重新计算,显示了脱气对混合物中溶解空气过饱和度的影响。 /span /em /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 根据该数据,在大气条件下,不会析出气体的混合物中空气的实际浓度为 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 38 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %,这是大多数脱气机设计要达到的目标(在特定仪表设计要求的流量和应用真空条件下)。 /span /p p span style=" margin: 0px padding: 0px line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 挑战当前的做法 /span /strong /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 今天,通常使用的在线脱气机使用管状 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " Teflon /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " & #8482 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " AF /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 或聚四氟乙烯( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " PTFE /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )膜。根据亨利定律,道尔顿定律和拉乌尔定律,它们允许空气通过膜脱离流动相。在恒定真空度下运行时,它们在低流速下更有效地从流动相中除去空气,而在高流速下则较少。这与在管子内的驻留时间相关。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 溶剂分子也可能从流动相移动到膜的真空侧。这种现象被称为渗透蒸发,在某些情况下以及某些 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 方法学中,这可以明显改变流动相的浓度。这是因为当真空固定在低于溶剂蒸气压的压力下时,泵将持续除去溶解的空气和溶剂蒸气。只要泵处于活动状态,溶剂供应瓶就会补充系统,并将溶剂蒸气泵入大气。因此,期望使用脱气机的真空侧来控制渗透蒸发,将压力设置为尽可能高而不会达到在 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统中将发生气体析出的点。 /span /p p span style=" text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 这会影响泵和入口单向阀的效率,并可能导致流动相组成和泵系统流速不准确,由于定量和鉴定问题,可能导致方法失败。 /span /p p span style=" margin: 0px padding: 0px line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 新 /span /strong /span strong style=" margin: 0px padding: 0px text-align: justify color: rgb(0, 82, 255) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 一代脱气技术 /span /strong /p section style=" margin: 0px 8px 0.1px padding: 0px text-align: justify color: rgb(51, 51, 51) text-transform: none line-height: 25.5px text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " strong style=" margin: 0px padding: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 任何新的脱气方法的理想设计特点应包括: /span /strong span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " /span /section ul class=" list-paddingleft-2" style=" list-style-type: disc " li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 流量限制比基于管式的脱气机低 /span /p /li li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 外形小巧,没有内部管件泄漏 /span /p /li li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 最低真空体积以限制挥发物的初始渗透蒸发 /span /p /li li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 恒定流阻,与施加的真空无关 /span /p /li li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 在可能的最高压力下对流动相进行脱气,而不会使流动相变得过饱和。在此称为 /span span style=" margin: 0px padding: 0px line-height: 21px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " “ /span span style=" margin: 0px padding: 0px line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 高压脱气 /span span style=" margin: 0px padding: 0px line-height: 21px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " ” /span span style=" margin: 0px padding: 0px line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " ,该技术减少或消除了溶剂蒸气向实验室空气的排放。 /span /span /p /li li p style=" margin: 0px 0px 0.1px padding: 0px line-height: 21px clear: both -ms-word-wrap: break-word !important min-height: 1em max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 脱气机已集成到 /span span style=" margin: 0px padding: 0px line-height: 21px font-family: Calibri, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " HPLC /span span style=" margin: 0px padding: 0px line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 系统控制软件中,可实现真空的智能控制,以确保提高脱气效率。 /span /span /p /li /ul p style=" text-align: center " img title=" 7.jpg" style=" max-height: 100% max-width: 100% " alt=" 7.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/d50a8504-53d9-4d48-b384-b02acafff1e0.jpg" / /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 此外,该脱气机的普适性(视 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统的类型而定,流速范围高达 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 10 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 并兼容所有常见溶剂,包括六氟异丙醇)将是一个显著的优势。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 现在,平面薄膜以及专用的真空泵控制算法可以实现这些目标。图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 2 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 显示了新型平面薄膜脱气机的示意图。这是一个简单的设计,可直接在低压和高压混合 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统中应用(图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 3 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )。该设计使产品具有最少的配件和连接。其高效膜具有足够的表面积,可用于分析型的 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统中的溶剂脱气(最高 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 10 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 流速)。独特的流道布局在泵的入口单向阀之前提供了较低的流体阻力。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 与之配套的真空控制算法可将其集成到分离方法控制协议中,并允许为任何 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统选择给定的脱气效率。真空压力可以调高或调低,以达到准确的 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 方法规范的需求。简化的界面依据 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 14.98px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 分离方法的流速和所需脱气效率,并将真空调节到高效脱气的尽可能的最高压力。该方法可防止溶解的空气过饱和,同时抑制渗透蒸发和流动相浓度变化。流阻是恒定的,与施加的真空无关。 /span /p p style=" text-align: center " img title=" 1.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/a56c5b4a-a6a3-4047-bb24-b0b374ee8a9d.jpg" / /p p style=" text-align: center " img title=" 2.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/378f7c09-44d9-45e7-8ae6-9da86c02c647.jpg" / /p p style=" text-align: center " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " em 图 /em /span em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 2. /span /em em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 新颖的流道设计, /span /em em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 薄液膜流过脱气膜。 /span /em /p p style=" text-align: center " img title=" 3.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/6cb7f6cc-2316-4d91-ada8-e29f01905f20.jpg" / /p p style=" text-align: center " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " em 图 /em /span em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 21px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 3. /span /em em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 集成到通用低压(左)和高压(右) /span /em em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 21px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " HPLC /span /em em style=" margin: 0px padding: 0px text-align: center color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 21px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 系统中的新型脱气机 /span /em & nbsp /p p span style=" margin: 0px padding: 0px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 在实践中 /span /strong /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 对新脱气机 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " / /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 控制算法的初步评估已产生了一些令人鼓舞的数据,并就可用性提出了积极的报告。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 为了表征脱气机,通过运行高效液相色谱分离得到了性能与应用真空度的数学模型,并将其存储在脱气机控制器或 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 控制系统中。第一步,是使用 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 210 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 纳米( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " nm /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )或 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 215 nm /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 下的甲醇 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " - /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 氧气电荷转移络合物来测定不同流速和应用真空下的脱气腔的效率。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 4 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 显示了在四个不同真空压力下效率与流速的关系。请注意,在 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 50 mmHg /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 下有 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 30 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %的残留空气(效率为 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 70 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %)时的最大流速约为 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 2.5 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 。这足以对高达 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 5 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 的梯度或任何等度流动相进行脱气,并且由于需要 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 62 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %的效率( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 38 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %的残留空气,图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 1 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )来防止气体析出,因此配备此脱气器的 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统在 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 50 mmHg /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 的压力下,可以预期使用高达 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 7 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 流速的方法而不会出现气泡。 /span /p p style=" text-align: center " img title=" 4.jpg" style=" max-height: 100% max-width: 100% " alt=" 4.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/c0e5cf48-96f7-42f8-a5e4-d71d6a7c126d.jpg" / /p p style=" text-align: center " span style=" margin: 0px padding: 0px font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " em span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 图 /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 4. /span span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 特征曲线显示了在四个不同真空度下薄膜脱气机的效率与流速的关系 /span /em /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 后续步骤绘制了每种流速的效率与真空度的关系曲线,并使用所需的效率和流速来求解效率 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " - /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 真空曲线方程式。每条曲线的公式将流速与输出真空水平联系起来,这样,一旦对脱气腔进行了表征,施加到脱气机上的真空水平就是该方法所需效率和流速的函数。然后可以使用真空控制来调节脱气性能,以覆盖 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " HPLC /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 系统的整个性能范围。因此,可以在任何流速下维持流动相最小的浓度变化(或渗透蒸发)始终确保目标脱气效率。 /span /p p span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 图 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 5 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 显示了比较平面薄膜和管式系统的脱气效率的实验数据。值得注意的是,真空水平明显不同,但是新型薄膜脱气机的性能在所需的流速( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 1 mL / min /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " )和效率( /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 70 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none line-height: 21px text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " %)上与管式脱气机相匹配。 /span /p p span style=" text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 这说明任何脱气器都可以被表征,然后可以将所得数据集用于根据效率和方法流速的输入来控制真空脱气系统。 /span /p p style=" text-align: center " img title=" 5.jpg" style=" max-height: 100% max-width: 100% " alt=" 5.jpg" src=" https://img1.17img.cn/17img/images/202004/uepic/7666a2d6-3f54-4ed1-997b-a09711f75123.jpg" / /p p span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong em 图 /em /strong /span strong style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " em style=" margin: 0px padding: 0px font-style: italic -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 5. /span /em /strong em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " 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-webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 50 mmHg /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 真空下,与标准的 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 18 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 英寸管式脱气机相比,在 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 1 mL / min /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 时的预计真空水平效率为 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 70 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px 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margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 流速下 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 70% /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 的效率时的预测真空度与标准 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 18 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 英寸管式脱气机在 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: Arial, sans-serif -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 50 /span /em em style=" margin: 0px padding: 0px text-align: left color: rgb(51, 51, 51) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(68, 114, 196) line-height: 14.98px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 毫米汞柱真空下的对比。 /span /em /p p span style=" margin: 0px padding: 0px line-height: 24px font-family: 宋体 font-size: 16px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 展望未来 /span /strong /span /p section style=" margin: 0px 8px 0.1px padding: 0px text-align: justify color: rgb(51, 51, 51) text-transform: none line-height: 25.5px text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 总而言之,与在恒定真空下进行脱气相比,此处描述的平面薄膜脱气机及其配套控制算法的发展为色谱工作者提供了更高的脱气性能。这些好处不仅将提高脱气效率,而且最重要的是,将提高方法的可重复性,实验室熟练度和生产率。 /span /section p span style=" text-align: left color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " /span span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " br/ /span /p p span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 您可以点击 /span a style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px text-decoration: underline -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " href=" https://www.instrument.com.cn/netshow/SH101586/" span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " https://www.instrument.com.cn/netshow/SH101586/ /span /a span style=" margin: 0px padding: 0px color: rgb(70, 70, 70) line-height: 21px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " & nbsp ,获取相关产品信息。或者给我们 400-860-5168转1586 留言,了解更多最新的技术。 /span /p p br/ /p p span style=" text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 参考文献: /span span style=" text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: Arial, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px float: none display: inline !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " Tokanuga J (1975) solubilities of oxygen,nitrogen and carbon dioxide in aqueous alcohol solutions, J Chem Eng Data,20(1): 41-46 /span /p p br/ /p p span style=" margin: 0px padding: 0px line-height: 24px font-family: 宋体 -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " strong span style=" color: rgb(0, 82, 255) " 关于作者 /span /strong /span /p p & nbsp span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " Carl Sims span class=" Apple-converted-space" & nbsp /span /span span style=" margin: 0px padding: 0px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 是 span class=" Apple-converted-space" & nbsp /span /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " IDEXHealth span class=" Apple-converted-space" & nbsp /span /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " & /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " Science span class=" Apple-converted-space" & nbsp /span /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 的首席科学家,专注于 /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " HPLC /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 系统的膜脱气,流体光学和 /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " UPLC /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 阀门 /span /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 微软雅黑, sans-serif font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " ins style=" margin: 0px padding: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " cite=" mailto:Zou,%20Cynthia" datetime=" 2020-03-24T12:35" 的研究 /ins 。在仪器领域拥有 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(70, 70, 70) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 47 /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif 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max-width: 100% box-sizing: border-box !important " HPLC /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " ,离子色谱, /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " Teflon AF /span span style=" margin: 0px padding: 0px font-family: 宋体 font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 光学以及 /span span style=" margin: 0px padding: 0px font-family: 微软雅黑, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " 早期职业生涯的 /span span style=" margin: 0px padding: 0px font-family: Arial, sans-serif font-size: 14px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important " DNA /span span style=" margin: 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text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 是在生命科学领域里流控和光学方面的权威专家。我们赋予客户三重优势,即借助我们的产品、人员和工程专业知识为您的光学和流路系统带来新的活力。 /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(91, 155, 213) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " IDEX Health & amp Science /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(91, 155, 213) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 提供完整的生命科学仪器研发的革新技术,用于分析仪器、临床诊断以及生物技术的应用。凭借行业内全面且先进的产品系列和工程能力, /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(91, 155, 213) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: -apple-system-font, BlinkMacSystemFont, " helvetica=" " pingfang=" " hiragino=" " sans=" " microsoft=" " yahei=" " font-size:=" " font-style:=" " font-weight:=" " word-spacing:=" " white-space:=" " -ms-word-wrap:=" " break-word=" " max-width:=" " box-sizing:=" " border-box=" " orphans:=" " widows:=" " background-color:=" " font-variant-ligatures:=" " font-variant-caps:=" " -webkit-text-stroke-width:=" " IDEX Health & amp Science /span span style=" margin: 0px padding: 0px text-align: justify color: rgb(91, 155, 213) text-transform: none text-indent: 0px letter-spacing: 0.54px font-family: 宋体 font-size: 14px font-style: normal font-weight: normal word-spacing: 0px -ms-word-wrap: break-word !important max-width: 100% box-sizing: border-box !important orphans: 2 widows: 2 background-color: rgb(255, 255, 255) font-variant-ligatures: normal font-variant-caps: normal -webkit-text-stroke-width: 0px " 参与到客户的需求中,提供最具生命力的解决方案,逐步成为光学及流控专家。可提供的产品有:连接件、阀门、泵、脱气机、空柱管、多岐管板、耗材、集成的流控组件、滤镜、镜头、快门,激光源,光引擎以及集成的光学组件。 /span /p p & nbsp /p p & nbsp /p p & nbsp /p

色谱脱气方法相关的方案

  • 智能脱气为原料药及辅料的比表面积测定提供保障
    在进行气体吸附实验或测定之前,必须清除固体样品表面及孔道中的水汽和杂质气等污染物。这个样品制备过程一般在真空加热的条件下进行,被称作脱气。由于脱气温度、脱气时间以及脱气真空度都与比表面积值有关,所以不同的脱气条件,会导致不同的 BET 比表面积结果。如何避免因样品处理引起的误差?你是否曾经为如何才算脱气完成而苦恼?你的MOF 或COF 样品是否因为脱气不当导致孔道坍塌?你的药品和辅料是否因为脱气温度过高导致分解?本文将为您解答这些疑问,抛弃这些烦恼。
  • 测量真空脱气率—— Pfeiffer Vacuum 真空系统解决方案
    许多前瞻性科技技术,例如粒子加速器、核聚变反应堆或 EUV 光刻技术都必须依赖高真空或超高真空。为了制造出这种持续的真空环境,并且维持在一定的真空度下,我们需要的不仅仅是能满足应用和技术规格的泵。同样重要的是需要在真空环境下对表面释放出的残余杂质进行精确的气体分析的仪器。然而,无论是设备的运营方,还是真空设备的制造商都需要仔细研究产品的特性、材料、及在真空环境中的表面处理和清洁方法。Pfeiffer Vacuum 丰富多样的产品组合为此类系统提供所有必要组件。Pfeiffer Vacuum 作为完整解决方案供应商为客户定制完美的残余气体分析设备。在残余气体分析中真空系统用于:■ 为高真空或超高真空选择合适的材料■ 检查电子构件、开关组和电缆在真空中的表现■ 评选适合的表面处理、镀膜合金材料■ 评估部件的清洗程序■ 检查真空烘烤程序■ 工艺控制Pfeiffer Vacuum 系统不仅为高真空和超高真空设备的运行方,还为真空部件的制造商提供优秀的残余气体分析解决方案。Pfeiffer Vacuum 也在本部使用残余气体分析,以便在开发和生产中测试其产品、表面处理和清洗程序的出气情况。以此确保 Pfeiffer Vacuum 产品适用于高真空和超高真空环境。此外,还可以检查涡轮分子泵的电机和前级真空部件的脱气状况。
  • 顶空气相色谱法分析变压器油中溶解气体
    本文采用岛津GC-2030气相色谱仪建立了顶空进样分析变压器油中溶解气体的分析方法。该方法灵敏度高,TCD检测器分析H2,方法检出限为30.28µ L/L;FID检测器分析C2H2,方法检出限为0.63µ L/L;重复性好,低烃RSD%3%;使用顶空进样器,省去脱气步骤,简单快速。

色谱脱气方法相关的资料

色谱脱气方法相关的试剂

色谱脱气方法相关的论坛

  • 流动相为什么要脱气?常用的脱气方法有拿几种?

    流动相为什么要脱气?常用的脱气方法有拿几种?流动相中溶解气体存在以下几个方面的害处 1、气泡进入检测器,引起光吸收或电信号的变化,基线突然跳动,干扰检测; 2、溶解在溶剂中的气体进入色谱柱时,可能与流动相或固定相发生化学反应; 3、溶解气体还会引起某些样品的氧化降解,对分离和分析结果带来误差。因此,使用前必须进行脱气处理。 常用的脱气法有以下几种:(1) 加热脱气法; (2) 抽吸脱气法 (3) 吹氦脱气法; (4) 超声波振荡脱气法。

  • 液相色谱流动相常用的脱气方法

    1. 吹氦脱气法 使用在液体中比空气溶解度低的氦气,在0.1Mpa压力下,以约60ml/min流速通入流动相10-15min以驱除溶解的气体。此法使用于所有的溶剂,脱气效果较好,但在国内因氦气价格较贵,本法使用较少;2. 加热回流法 此法的脱气效果较好;3. 抽真空脱气法 此时可使用微型真空泵,降压至0.05-0.07MPa即可除区溶解的气体。显然使用水泵连接抽滤瓶和G4微孔玻璃漏斗可一起完成过滤机械杂质和脱气的双重任务。由于抽真空会引起混合溶剂组成的变化,故此法适用于单一溶剂体系脱气。对多元溶剂体系应预先脱气后再进行混合,以保证混合后的比例不变。4. 超声波脱气法 它是目前实验室使用最广泛的脱气方法,将配制好的流动相连同容器一起放入超声波水漕中脱气10-20min即可。该方法操作简便,基本能满足日常分析的要求。5. 在线真空脱气法 把真空脱气装置串联到储液系统中,并结合膜过滤器,实现了流动相在进入输液泵前的连续真空脱气。此法的脱气效果明显优于上述几种方法,并适用于多元溶剂体系。

色谱脱气方法相关的耗材

  • 脱气工具包
    产品名称:脱气工具包仪器厂商:PerkinElmer/美国 珀金埃尔默价格:面议库存:是使用溶剂脱气系统能提高您泵的性能。PerkinElmer提供真空脱气系统来满足您的脱气需求。200系列在线真空脱气机工具包这是一个体积小,效率高的在线模块,可以将溶解气体从液相色谱溶剂中除去。该真空脱气机有3通道和5通道两种型号可供选择,来支持等度、二元和四元泵以及自动进样器洗针溶剂的脱气。使用溶剂脱气系统能提高您泵的性能。PerkinElmer提供真空脱气系统来满足您的脱气需求。说明零件编号3通道真空脱气工具包包括1个真空脱气机、1个带瓶盖的1L瓶、1个带瓶盖的2L瓶、1个溶剂托盘和附件N26005715通道真空脱气工具包包括1个真空脱气机、1个带瓶盖的1L瓶、2个带瓶盖的2L瓶、溶剂托盘N2600570双瓶盖工具包包括2个溶剂瓶所需要的2个瓶盖、管路、配件和标签N2600522四瓶盖工具包包括4个溶剂瓶所需要的4个瓶盖、管路、配件和标签N2600523
  • 溶剂过滤器/脱气器
    产品特点: 溶剂过滤器/脱气器 过滤溶剂的另一个优点是同时进行了脱气。如果您的系统中没有在线脱气机,则此优点尤其显著。溶剂过滤的优点是: &bull 对洗脱液进行脱气,去除颗粒 &bull 防止检测器内形成假峰,这是由于色谱的低压端的溶剂气泡造成的 &bull 延长溶剂入口寿命 &bull 避免因检查阀中的气穴和微粒造成泵停止运行 &bull 减少柱塞杆磨损,延长柱寿命 订货信息: 溶剂过滤器/脱气器     说明     部件号 HPLC 溶剂过滤器/脱气器组件 3150-0577 可更换的部件用于3150-0577 玻璃漏斗,250 mL 5188-2743 PTFE 涂层筛网 5188-2744 PTFE 密封垫 5188-2745 漏斗底座,玻璃 5188-2746 溶剂过滤系统 5067-0215 可更换的部件用于5067-0215 可更换的烧瓶,1 L 5067-0216 底座 5067-0217 漏斗 5067-0224 滤膜 再生纤维素过滤器滤膜47/45,100/包 3150-0576 尼龙滤膜47/45,100/包 9301-0895 PTFE 过滤器滤膜47/45,10/包 3150-0509
  • 在线脱气装置SHT-5
    SHT-5型是一款可实现多通道脱气的在线脱气装置,采用连续式抽真空模式,脱气效率更加持续和稳定,可以用于液相色谱、离子色谱等设备的流动相在线脱气。可满足四通道的拓展需求,智能屏幕实时显示仪器参数及性能状态。
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