德国迈克(Dr.maisch)色谱柱选择
德国迈克Dr.Maisch色谱柱分类包括: 图34 图34:Nanocolumns,纳米微径柱,微径色谱柱纳米微径管液相色谱柱用纳升微径色谱柱可以非常方便的提高物质分离的灵敏度和检测限, 可以提高5000个基数点比普通的4.6内径的柱子.1.)规格: 150 mm x 75 μm类型: Reprosil-Pur C18-AQ, 3 μm货号.: R13.aq.s150.075 批次.: 120305 86401流动相: 乙腈 /水 (70 /30) 流速: 200 nl / min.柱压: 90 bars检测波长: UV 254 nm结果分析:Peak 1: Nitrobenzene , RT 2.96 min. N/m = 70 000Peak 2: Biphenyl, RT 6.8 min.N/m = 120 000 2.)规格: 200 mm x 75 μm类型: Reprosil-Pur 300 ODS-3, 3 μm货号.: R33.93.s200.075 批号.: 280905 16001流动相:乙腈 /水 (70 /30)流速: 200 nl / min.压力: 100 bars检测器: UV 254 nm 结果分析:Peak 1: Nitrobenzene, RT 4.65 min. N/m = 54 000Peak 2: Biphenyl, RT 7.9 min. N/m = 95 000 如果想增加竹子的检测灵敏度,可以把柱子的内径变得更小Column-id (mm)Flow(μl/min)Increase of Sensivity4.6100012.020041.040210.510850.332350.10.521000.0750.33760Fused Silica capillary columns with50 μm, 75 μm, 100μm, 150 μm idStainless steel GLT-columns with0.3mm0.4mm 0.5mm 0.75mm id Reprosil-Pur C18-AQ 3um长度40mm125mm150mm200mm250mm内径0.75mm--0.050mm,其他长度可以另询3750元3900元`4200元4400元4600元可以提供各种填料类型的,各种规格内径长度的微径液相色谱柱,如有疑问请致电上海宸乔生物科技有限公司。 图35 图35:U-HPLC (Maisch) 超高压液相色谱柱描述碳含量Mat. No.ReprospherReprospher 100 C18, 1.8 μm16%endc.rs118.9e.Reprospher 100 C18, 2 μm16%endc.rs12.9e.Reprospher 100 C18, 2.5 μm16%endc.rs125.9e.Reprospher 100 C18-DE, 1.8 μm16%double endc.*rs118.9de.Reprospher 100 C18-DE, 2 μm16%double endc.*rs12.9de.Reprospher 100 C18-DE, 2.5 μm16%double endc.*rs125.9de.Reprospher 100 C18-Aqua, 1.8 μm12%pol.Gr.+ endc.rs118.9aq.Reprospher 100 C18-Aqua, 2 μm12%pol.Gr.+ endc.rs12.9aq.Reprospher 100 C18-Aqua, 2.5 μm12%pol.Gr.+ endc.rs125.9aq.Reprospher 100 C18-NE, 1.8 μm15%not endc. rs118.90.Reprospher 100 Phenyl, 1.8 μm9%double endc.*rs118.pde.Reprospher 100 Phenyl, 2 μm9%double endc.*rs12.pde.Reprospher 100 Phenyl, 2.5 μm9%double endc.*rs125.pde.Reprospher 100 C8-Aqua, 1.8 μm8%pol.Gr.+ endc.rs118.8aq.Reprospher 100 C8-Aqua, 2 μm8%pol.Gr.+ endc.rs12.8aq.Reprospher 100 C8-Aqua, 2.5 μm8%pol.Gr.+ endc.rs125.8aq.Reprospher 100 C8, 1.8 μm10%endc.rs118.8e.Reprospher 100 C8, 2 μm10%endc.rs12.8eReprospher 100 C8, 2.5 μm10%endc.rs125.8eReprospher 100 C8-DE, 1.8 μm10%double endc.*rs118.8de.Reprospher 100 C8-DE, 2 μm10%double endc.*rs12.8de.Reprospher 100 C8-DE, 2.5 μm10%double endc.*rs125.8de.Reprospher 100 CN, 1.8 μmrs118.C0*Modified with 2 endcappings: the first endcapping takes place in the liquid-form and the second additional endcapping takes place in gas-form, which makes the phases much more base deactivated than conventional single step endcapping techniques. These phases are more "inert" and more pH stable than those manufactured using with conventional endcapping techniques.ReproSil-SaphirReprosil Saphir 100 C18, 1.8 μm20%endc.ra118.9eReprosil Saphir 100 C18 , 2.2 μm20%endc.ra122.9eReproSil-Pur BasicReprosil-Pur Basic 120 C18, 1.9 μm17 % Cdouble bound endc.r119.b9.Reprosil-Pur Basic 120 C18, 2.5 μm17 % Cdouble bound endc.r125.b9.ReproSil-PurReproSil-Pur 120 C18-AQ, 1.9 μm15 % Cendc.r119.aqReproSil-Pur 120 C18-AQ, 2.4 μm15 % Cendc.r124.aq.ReproSil-Gold Turbo 图36 图36:ReproGel (Maisch) 糖和有机酸分析柱规格型号: 250 x 8 mm oder 300 x 8 mm iD.适合分析糖,有机酸,氨基酸等物质规格型号: 250 x 8 mm or 300 mm x 8 mm ,其他规格型号可以来电询问. 型号应用方面流动相体系编号对应美国药典ReproGel H, 9 μmfor sugars,alcohols and acidsWater or 9mM sulfiric acidsu9.h0L-17ReproGel Ca, 9 μmfor sugars and alcoholsWater at 80 C°su9.ca.L-19ReproGel Na, 9 μmfor sugarsWater at 80 C°su9.na.L-58ReproGel Pb, 9 μmfor sugarsWater at 80 C°su9.pb.L-34ReproGel Ag, 9 μmfor sugarsWater at 80 C°su9.ag.References of ReproGel H+ References of ReproGel Ca2+ References of ReproGel Pb2+ Organic acids: ReproGel-H, 9 μm (250 x 8 mm)Eluent: 9 mM SulfuricAcid, Flow rate: 1 ml/min.,Det.: 210 nm Red Wine: ReproGel-H,9 μm (250 x 8 mm)Eluent: Water, Flow rate: 0,7 ml/min. Temperature: 25 C°, Injection: 20 μl. Acids are retained with 20 x 4.6 mm SAX-Guard-Column. ReproGel-Ca, 9 μm (250 x 8 mm)Eluent: H20Flow rate: 0,5 ml/min.Temperature: 80 C°,Detection: RI,Pressure: 35 bar Lactose:ReproGel-Ca,9 μm (250 x 8mm)Eluent: water,Flow rate: 0,3 ml/minTemperature: 80 C°Detection: RI ReproGel-Ca, 9 μm, (250 x 8 mm)Flow rate: 0,5 ml/minTeperature.: 80 C°Detection: RIInjection: 20 μl Sugars: ReproGel-Pb,9 μm (250 x 8 mm,)Eluent: H20, Flow rate: 0,3 ml/min.,Temperature: 80 C°,Detection: RI, Pressure: 25 bar 图37 图37:Reprosil Chiral 手性色谱柱 德国Dr.maisch公司的手性色谱柱种类非常丰富,并且性价比非常高,各种型号的分析和制备柱均可提供,在欧洲国家使用非常广泛。描述美国药典对应编号备注Reprosil Chiral-OM(USP-L40) 与大赛璐公司OD系列相对应Reprosil Chiral AM(USP-L51) 与大赛璐公司AD系列相对应Reprosil Chiral-NR&ReproSil Chiral-NRR ReproSil Chiral-NR 与 ReproSil Chiral-NRR色谱柱之间您可以随意的切换流动相,使用起来非常方便。这个色谱柱非常适合有芳香物质中O原子接近手性中心的物质拆分。- Chiral NR/AM/OM -三个色谱柱的相比较Reprosil Chiral-AA ReproSil手性-AA是专为未衍生氨基酸的手性分离。这一阶段还显示了对恶唑烷酮,海因,二氮杂亚砜和良好的选择性。 它是基于超纯Reprosil100二氧化硅。用手性选择剂:芳香族化合物,共价结合到一个8微米的二氧化硅微球Reprosil Chiral-OH 该Reprosil手性-OH是专为芳香酒精化合物的手性分离。OH基团共价结合于超纯Reprosil100二氧化硅。最成功分离的手性化合物是: 1)芳香族化合物 2)具有OH基的手性中心。Reprosil Chiral-PS 手性ReproSil-PS是专为手性芳族化合物,它含有P或S原子的分离Reprosil Chiral-CA ReproSil手性-CA是专为手性芳香羧酸的分离。 Reprosil Chiral-AMS与大赛璐AS-H色谱柱相对应Reprosil Chiral-CM 与大赛璐OC-H色谱柱相对应Reprosil Chiral-JM 与大赛璐OJ-H色谱柱相对应Reprosil Chiral-ZM 与大赛璐OZ-H色谱柱相对应Reprosil Chiral-ZA 与Epitomize 1K色谱柱相对应Reprosil Chiral-YM 与大赛璐AY-H色谱柱相对应Reprosil Chiral-BM 与大赛璐OB-H色谱柱相对应Reprosil -AGP(USP-L41)Reprosil-HSAReproSil Chiral-TAG USP-L63适合分析Aminoalkohols,N-阻断氨基酸,α-羟基酸,Oxazolidinons,海因,酰亚胺,氨基酸类 Reprosil Chiral-TG 适合分析芴甲氧羰酰基 和丹磺酰氯保护的氨基酸Reprosil Chiral CD USP-L45 USP-L45(丹酰-氨基酸,巴比妥类,普萘洛尔,磺胺类药物,Prostaglandines)Reprosil Chiral-D-PhenylGlycin(USP-L36) 刷型 D-苯基甘氨酸,适合分析 布比卡因Reprosil Chiral-l-Prolin(USP-L32) Reprosil手性-L-脯氨酸,5微米° 对于DL-Atrolactinacid,DL-扁桃酸,DL-乳酸,DL-天冬酰胺 DL-塞林,DL-苯丙氨酸,DL-苏氨酸,DL-脯氨酸,DL-组氨酸,625, - DL-华菱,DL-酪氨酸,DL-色氨酸可以很好的分析。 图38 图38:ReproSil 70/100/300 系列色谱柱 多孔球状二氧化硅:3,5,10微米 孔径:70 A°/500平方米/克,100 A°/280平方米/克,300 A°/100平方米/克 孔体积:0.9,1.1毫升/克 性价比最高的色谱柱,非常适合做制备,稳定的重复性和低压的设计。References of ReproSil 70 C18 References of ReproSil 100 C18 References of ReproSil 100 C8 References of ReproSil 100 ODS-A References of ReproSil 100 Phenyl References of ReproSil 300 C18 描述碳含量封尾编号ReproSil 70 Si, 5 μmr05.06.ReproSil 70 C18, 3 μm20 % Cendc.r03.96.ReproSil 70 C18, 5 μm20 % Cendc.r05.96.ReproSil 70 C8, 5 μm14 % Cendc.r05.86.ReproSil 70 C4, 5 μm10 % Cendc.r05.46.ReproSil 70 Phenyl, 5 μm16 % Cendc.r05.pe.ReproSil 70 CN, 5 μm10 % Cendc.r05.c6.ReproSil 70 Diol, 5 μm4 % Cr05.d6.ReproSil 70 NH2, 5 μm5 % Cr05.a6.with 100A° poresReproSil 100 Si, 3 μmr13.06.ReproSil 100 Si, 5 μmr15.06.ReproSil 100 Si, 10 μmr10.06.ReproSil 100 C4, 3 μm5 % Cendc.r13.46.ReproSil 100 C4, 5 μm5 % Cendc.r15.46.ReproSil 100 C4, 10 μm5 % Cendc.r10.46