This Application Note shows the transfer of a standard HPLC method to a UHPLC method for the analysis of 13 DNPH-derivatized aldehydes and ketones. By transferring the method from HPLC to UHPLC, the analysis time and solvent consumption was reduced by approximately 90 %. The results demonstrate the benefi t of transferring an HPLC method to UHPLC conditions without compromising precision, linearity, or limits of detection and quantifi cation.
采用吹扫捕集技术(Punge and Trap lechnique)对不同十字花科蔬菜中的挥发性成分进行了富集,以气质联用仪(GC/MS)进行鉴定。结果在白菜、羽衣甘蓝、芥蓝、青花菜、芥菜和大白菜中共鉴定出86 种挥发性物质,化合物的种类包括醇类、醛类、酮类、酯类、硫醚类等,同时还发现了硫苷降解产物异硫氰酸盐和腈类等化合物。