The medicinal plant Atractylodes macrocephala (Baizhu in Chinese) has been widely used in traditional Chinese medicine for energy and stomach complaints, treatment of dyspepsia and anorexia, anti-inflammation, anticancer and for increasing assimilation.A high-speed counter-current chromatography (HSCCC) method was developed for the preparative separation and purification of two main bioactive components,namely, atractylon and atractylenolide III from A. macrocephala by using light petroleum (60–908C)–ethyl acetate–ethanol–water (4 :1:4:1 v/v) as the two-phase solvent system in dual-mode elution. Compared with the separation using the normal-mode elution, the dual-mode HSCCC can be achieved with shorter elution time.Atractylenolide III (32.1 mg) at 99.0% purity and 319.6 mg atractylon at 97.8% purity could be obtained from 1000 mg crude sample in a single run. The recoveries of atractylenolide III and atractylon were 95.4 and 92.6%, respectively.
【目的】研究磷酸盐用量对僵直前猪肉、成熟猪肉和冻猪肉制成的乳化肠贮藏期间保水和质构性质的影响。【方法】僵直前肉、成熟肉和冻肉分别用5 个浓度梯度的磷酸盐进行预混合,并制作乳化肠。利用质构仪、压力仪测定乳化肠刚产出时的产率、硬度、总压出汁液和贮藏至10 d、20 d 及30 d 的硬度及贮藏损失。【结果】僵直前肉制作的乳化肠与成熟肉和冻肉制作的乳化肠相比,产率高,贮藏期间硬度增加小。【结论】僵直前原料肉可提高乳化肠的保水和质构性质。在较高的NaCl 使用量(3%)下,单纯增加磷酸盐的使用量并不能解决乳化肠贮藏期间保水和质构问题。