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产品介绍
产品特点:
5400B Thermal Transfer System
The analysis of adsorbent tubes can be a nightmare for analytical laboratories,especially when there is a requirement to get results on 100% of the tubes tested. Instrument problems, unexpected analyte loading outside of the GCMS calibrated range, and cross-contamination make the normal “one-shot” analysis very risky. Even attempting to recover a “split” fraction of the tube sample into another tube is plagued with problems such as added background, poor leak-free validation, and incomplete recoveries from yet a second tube.
The 5400B Thermal Transfer System simplifies the entire thermal desorption tube analysis process. The 5400B automates the precise transfer of tube samples into vacuum-tight Bottle-Vac samplers. During desorption, approximately 600cc of nitrogen is used to recover the tube sample much more completely than direct GC thermal desorbers – which attempt to desorb the sample using as little helium as possible.
The 5400B performs an automated leak check before thermally desorbing the tube sample to ensure quantitative sample recovery.After desorption, final pressure is adjusted to obtain the same desorption volume for each sample transfer. Once the sample is transferred into a Bottle-Vac, as little as 0.1–1.0cc of the sample can be analyzed, or the entire volume using a 7200 or 7200 / 7650. Further dilutions are also easily accomplished.
Features
● Sample Screening
● Perform Multiple Analyses
● Increase Dynamic Range
Optimize the resolution of your GCMS for quantitative analysis.
● Tube / Canister Shared Calibration
Reliable and simplified GCMS analysis.
● Flexible Conguration
Easily customize your 5400 to handle multiple tube sizes.
● Flow Rate Control
Control desorption flow rate to optimize recovery.
● Leak Checking
New, low volume pressurized leak check eliminates potential for sample loss.
● High Temperature Operation
New, high temperature operation to 340?C for improved high molecular weight recovery for Method TO-17.
● Complete Software Control
Improved Windows software with an advanced and intuitive user interface.
● Bakeout Mode
New bakeout mode for TD Tube Thermal Conditioning.
● Radiello TD Tube Analysis
Supports analysis of Radiello thermal desorption cartridges
订购信息:
DESCRIPTION | PART # | UNIT |
5400B Thermal Transfer System* | 5400B | EA |
Heater - 6mm OD x 11.5cm (Supelco, Dynatherm) | 09-25010 | EA |
Heater - 1/4” OD x 7” (Tekmar, Gerstal) | 09-25020 | EA |
Heater - 1/4” OD x 3.5” (Perkin-Elmer, Markes, Entech) | 09-25030 | EA |
Heater - 5/8”OD x 5” (VOST, 1/4”ends) | 09-25070 | EA |
Female Micro-QT / Tube Fitting | FQT-400VLS | EA |
3/16” Radiello Desorber Tube | 36-54100B | EA |
SVOC Preparation Tube | 36-54200 | EA |
*Heaters are not included with base unit. | ||
Order heaters separately and configure as needed. |
1 Attach trap heater onto 5400B assembly. | 2 Attach other trap heaters as needed. |
3 Attach Micro-QT fitting onto desorbtion tube. | 4 Insert tube with fitting into tube heater. |
5 Gently snug thumb-wheel on bulkhead fitting and perform pressurized leak check. | 6 Attach an evacuated container to the top. |
供应商
银牌会员 第16年