null检测 | 中国客户在国际期刊上发表的文章：Synthesis of conducting polyaniline using novel anionic Gemini surfactant as micellar stabilizer-北京东方德菲仪器有限公司

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The Gemini surfactant 9B-4-9B containing sodium sulfonate as hydrophilic head group was synthesized based on nonylphenol and characterized by FTIR, 1H NMR spectroscopy and the surface tension measurement. The CMC and C20 of the 9B-4-9B were smaller than that of sodium dodecylbenzene sulfonate and sodium dodecylsulfate, respectively, indicating excellent efficiency of micelle formation and reduced surface tension. Conducting polyaniline salts were synthesized by chemical oxidative micellar polymerization of aniline in water firstly using Gemini surfactant 9B-4-9B as the micelle stabilizer and ammonium peroxydisulfate as the oxidant at 0 C. The stable polyaniline dispersions have been obtained when the molar ratio of the 9B-4-9B to aniline was equal to or above 0.5 used in the polymerization system. The obtained granular polyaniline particles with the size of 1–2 lm were characterized by FTIR, UV–Vis, SEM, WAXD and conductivity measurement.

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