调制DSC的条件的选择

2016/03/21   下载量: 19

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应用领域 电子/电气
检测样本 其他
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Modulated DSC is a powerful tool for materials characterization. Like any other precision technique, failure to use the optimum experimental conditions can result in sub-par performance. Following the suggestions listed in this paper should help you to design your MDSC experiment so that you derive the highest quality data.

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INTRODUCTION

Modulated DSC (MDSC®) provides a powerful enhancement to the standard DSC experiment. MDSC can simultaneously improve the sensitivity and resolution of the DSC experiment, in addition to providing heat capacity and heat flow in a single experiment. In order to obtain the maximum benefit from the MDSC experiment, however, optimal MDSC conditions must be chosen. In this paper we examine the protocol for choosing the correct MDSC conditions with respect to sample size, modulation period, underlying heating rate, and modulation amplitude.


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