NiB的XRDtu
NiB的XRD图
liuhz1 发表:我想知道各个峰的归属，因为以前从来没做过，所以有很多很简单的问题一不懂。比如说有没有比较简单的方法知道各个峰的归属。那个卡片该怎么查啊，我也没怎么看懂啊，对了还应该有他们的数据
File: LB.DI 30-Sep-2006 11:41
==============================================================================
Philips Analytical PC-APD, Diffraction software
Sample identification: lb
Data measured at: 30-Sep-2006 10:48:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 [廬: 1.54060
Wavelength Alpha2 [廬: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1?
Receiving slit: 0.3
Monochromator used: NO
Start angle [?閉: 10.000
End angle [?閉: 80.000
Step size [?閉: 0.100
Maximum intensity: 13087.36
Time per step : 4.000
Type of scan: STEP
Minimum peak tip width: 0.00
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.75
Number of peaks: 20
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[?閉 ? [廬 ? [廬 [?閉 [counts] [counts] [%]
29.325 3.0432 3.0506 0.700 259 6225 2.0 1.42
36.630 2.4513 2.4573 0.500 1714 6626 13.1 2.39
37.680 2.3854 2.3912 0.400 4502 6642 34.4 6.04
39.060 2.3042 2.3099 0.300 2304 6659 17.6 1.23
39.780 2.2642 2.2697 0.400 2884 6675 22.0 2.26
42.160 2.1417 2.1469 0.400 5580 6691 42.6 4.37
43.705 2.0695 2.0746 0.400 8668 6708 66.2 1.17
44.290 2.0435 2.0485 0.300 13087 6724 100.0 4.29
45.500 1.9919 1.9968 0.400 10424 6740 79.7 10.26
46.455 1.9532 1.9580 0.300 7413 6740 56.6 3.46
48.785 1.8652 1.8698 0.600 6053 6773 46.2 12.09
51.080 1.7867 1.7910 0.400 2314 6806 17.7 2.00
52.560 1.7398 1.7441 0.300 2725 6823 20.8 1.70
54.150 1.6924 1.6965 0.300 1384 6839 10.6 0.96
55.020 1.6677 1.6718 0.300 708 6856 5.4 1.16
56.565 1.6257 1.6297 0.600 1102 6872 8.4 3.32
61.870 1.4984 1.5021 0.800 225 6464 1.7 0.94
65.005 1.4336 1.4371 0.400 135 6320 1.0 0.76
72.470 1.3032 1.3064 0.500 762 6241 5.8 2.29
75.780 1.2543 1.2573 0.300 625 6320 4.8 1.43
ile: LH.DI 30-Sep-2006 11:44
==============================================================================
Philips Analytical PC-APD, Diffraction software
Sample identification: lh
Data measured at: 30-Sep-2006 9:54:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 [廬: 1.54060
Wavelength Alpha2 [廬: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1?
Receiving slit: 0.3
Monochromator used: NO
Start angle [?閉: 10.000
End angle [?閉: 80.000
Step size [?閉: 0.100
Maximum intensity: 1857.610
Time per step : 4.000
Type of scan: STEP
Minimum peak tip width: 0.00
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.75
Number of peaks: 5
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[?閉 ? [廬 ? [廬 [?閉 [counts] [counts] [%]
12.010 7.3632 7.3813 0.600 520 5344 28.0 1.04
32.925 2.7182 2.7249 0.600 1858 6178 100.0 5.54
43.985 2.0570 2.0620 1.000 681 8892 36.7 1.66
59.130 1.5612 1.5650 0.600 1011 5715 54.4 2.91
65.025 1.4332 1.4367 0.500 292 4886 15.7 1.14
这是一些参数下面一个对应第一个图
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