nalysis of Semivolatile Organic Compounds Using Hydrogen Carrier Gas and the Agilent HydroInert Source by Gas Chromatography/Mass Spectrometry

2024/02/22   下载量: 1

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Abstract Gas chromatography/mass spectrometry (GC/MS) is integral to the analysis of semivolatile organic compounds (SVOCs) in environmental matrices. Recent pressure on the helium (He) supply has required organizations to actively investigate hydrogen (H2) carrier gas, but most GC/MS analyses have reduced sensitivity and hydrogenation or dechlorination in the sources. The Agilent HydroInert source retains the ability to analyze a wide calibration range (0.1 to 100 μg/mL) and meet the U.S. Environmental Protection Agency (EPA) method 8270 calibration criteria when using H2 carrier gas.

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Introduction


GC/MS is regarded as the select analytical technique for the analysis of SVOCs. Governmental regulatory authorities have established methods and performance criteria for the measurement of SVOCs identified as pollutants in nvironmental and industrial matrices. For example, the U.S. EPA method 8270 (versions 8270D and 8270E) contains a list of over 200 compounds suitable for analysis by GC/MS in solid waste, soil, air, and water extracts.1,2 Method 8270 contains SVOCs across several analyte class types from acids, bases, neutral compounds, and polyaromatic hydrocarbons (PAHs); this method also has detailed specifications and requirements for the Quantitative Analysis of SVOCs


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