方案摘要
方案下载应用领域 | 环保 |
检测样本 | 空气 |
检测项目 | 有机污染物>多环芳烃类化合物 |
参考标准 | / |
Using the Agilent HydroInert source in a challenging soil matrix
Abstract
The Agilent 8890 GC and 7000E triple quadrupole GC/MS system (GC/TQ) with a novel electron ionization (EI) source—the Agilent HydroInert source, which is optimized for hydrogen carrier gas—were used for the analysis of polycyclic aromatic hydrocarbons (PAHs). The optimized method using the HydroInert source provides excellent peak shape, sensitivity, and linearity of R2 ≥0.999, which was observed for all 27 analytes over their respective calibration ranges (0.1 to 1,000 pg for 26 analytes and 0.25 to 1,000 pg for one analyte). Method detection limits (MDLs) ranged from 0.03 to 0.16 pg with an average of 0.09 pg. The stability of calculated concentrations over 500 injections is presented, where, with routine maintenance and backflush, injection RSDs were <12% for all analytes. Further, the ability of the Agilent universal Ultra Inert (UI) mid-frit inlet liner to handle a complex matrix is demonstrated. By proper selection of instrument configuration and operating conditions, the system with hydrogen carrier gas can generate results comparable to or better than those with helium.
使用 Agilent InfinityLab 在线液相色谱 系统实现对流动化学反应器中反应过 程的实时监测
使用配备氦气节省模块以进行载气 切换的 Agilent 8850 气相色谱系统 分析香草提取物的方法转换
应用 QuEChERS 方法结合 Agilent 7000 系列三重四极杆气质联用仪测定甜菜中 的多农药残留
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