下面是NMR法测定绝对构型的一些文献资料,基本上都是影响比较大的杂志发表的,经典工作.供同志们参考. Selected Publication List on Methods for the Determination of Absolute Configurations by NMR
J.M. Seco, Sh. Latypov, E. Quiñoá and R. Riguera "The determination of the absolute stereochemistry of alcohols by low temperature H-NMR of Arylmethoxyacetates." Tet. Asymmetry, 1995, 6, 107
Sh. Latypov, J.M. Seco, E. Quiñoá and R. Riguera "Conformational structure and dynamics of Arylmethoxyacetates: DNMR spectroscopy and aromatic shielding effect." J. Org. Chem., 1995, 60, 504-515
Sh Latypov, J.M. Seco, E. Quiñoá and R. Riguera "Determination of the absolute stereochemistry of chiral amines by H NMR of Arylmethoxyacetic acid amides: The conformational model." J. Org. Chem., 1995, 60, 1538-1545
M.J. Ferreiro, Sh Latypov, E. Quiñoá and R. Riguera "Determination of the absolute configuration and enantiomerical purity of chiral primary alcohols by H NMR of 9-Anthrylmethoxyacetates." Tet. Asymmetry, 1996, 7, 2195-8
Sh. Latypov, J. M. Seco, E. Quiñoá and R. Riguera "MTPA vs MPA in the determination of the absolute configuration of chiral alcohols by H-NMR." J. Org. Chem., 1996, 61, 8569-8577
M. J. Ferreiro, Sh. Latypov, E. Quiñoá and R. Riguera. "The use of Ethyl 2-hydroxy-2-(9-anthryl) acetate for Assignment of the Absolute Configuration of Chiral Carboxylic Acids by 1H NMR." Tet. Asymmetry, 1997, 8(7), 1015-1018
J. M. Seco, Sh. Latypov, E. Quiñoá and R. Riguera "Determining factors in the assigment of the Absolute Configuration of Alcohols by NMR: The use of anysotropic effect at Remote positions." Tetrahedron, 1997, 53, (25), 8541-8564
M. Fernández, L. Muñoz, R. Fernández and R. Riguera "Asymmetric synthesis of the b-aminoacid methyl ester derivative of Onchidin: (2S,3S)-Methyl-3-Amino-2-Methyl-7-Octynoate and its enantiomer." Tet. Asymmetry, 1997, 8, (11), 1847-1854
J. M. Seco, Sh. Latypov, E. Quiñoá and R. Riguera "Choosing the right reagent for the determination of the Absolute Configuration of amines by NMR: MTPA or MPA?." J. Org. Chem., 1997, 62,7569-7574
Sh. Latypov, M.J. Ferreiro, E. Quiñoá and R. Riguera "The Assignment of the Absolute Configuration of b-Chiral Primary Alcohols by NMR: Scope and Limitations." J. Am. Chem. Soc., 1998, 120, 4741-4751
Sh. Latypov, J. M. Seco, E. Quiñoá and R. Riguera "Are Both the (R)- and the (S )-MPA Esters Really Needed for the Assigment of the Absolute Configurarion of Secondary Alcohols by NMR? The use of a single derivative." J. Am. Chem. Soc., 1998, 120, 877-882
Sh. Latypov, Ricardo Riguera, Michael B.Smith and Jana Polivkova "Conformational analysis of 1-(alkoxymethyl)-5R-methyl-2-pyrrolidinone derivatives Determination of the Absolute Configuration of Alcohols." J. Org. Chem., 1998, 63, 8682-8688
J. M. Seco, E. Quiñoá and R. Riguera 9-Anthrylmethoxyacetic Acid Esterification shifts. A Correlation with the Absolute Stereochemistry of Secondary Alcohols." Tetrahedron, 1999, 55, 569-584
J. M. Seco, E. Quiñoá and R. Riguera. "Boc-Phenylglycine: the Reagent of Choice for the Assignment of the Absolute Configuration of a-Chiral primary Amines by 1H-NMR" J. Org. Chem., 1999, 64, 4669-4675
B. López, E. Quiñoá and R. Riguera "Complexation with Barium(II) Allows the Inference of the Absolute Configuration of Primary Amines by NMR." J. Am. Chem. Soc., 1999, 121, 9724-9725
Commentary in Chemical & Engineering News, 1999, October 25, p. 37.
M. J. Ferreiro, SH. K. Latypov, E. Quiñoá and R. Riguera "The Assignment of the Absolute Configuration of Carboxylic Acids by 1H NMR Spectroscopy." J. Org. Chem., 2000
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