【分享】一本关于NMR弛豫的专著 Practical NMR relaxation for chemists [PDF,209p]

Contents ...
Contents vii
4.3 Intermolecular Dipole–Dipole Interactions 53
4.4 Electric Field Gradients
at Quadrupolar Nuclei 53
4.5 Nuclear Quadrupole Coupling Constant
as Measure of the Electric Field Gradient 54
4.6 Quadrupole Relaxation 56
Bibliography 57
5 Relaxation by Chemical Shift
Anisotropy, Spin–Rotation
Relaxation, Scalar Relaxation
of the Second Kind
and Cross-mechanisms 59
5.1 Relaxation by Chemical Shift Anisotropy 59
5.2 Spin–Rotation Relaxation 63
5.3 Interference Mechanisms of Nuclear Relaxation 64
5.4 Scalar Relaxation of the Second Kind 65
Bibliography 67
6 Nuclear Relaxation in Molecular
Systems with Anisotropic Motions 69
6.1 Spin–Lattice Nuclear Relaxation in Ellipsoidal
Molecules: Temperature Dependences
of T1 Times 70
6.2 How to Reveal Anisotropic Molecular Motions
in Solution 74
viii Contents
6.3 Nuclear Relaxation in the Presence
of Correlation Time Distributions 76
Bibliography 80
7 1H T1 Relaxation Diagnostics
in Solution 81
7.1 Revealing Weak Intermolecular Interactions
by T1 Time Measurements in Solution 82
7.2 T1 Studies of Exchange in Simple Molecular
Systems 87
7.3 Structural 1H T1 Criterion 89
7.4 Partially Relaxed NMR Spectra 92
Bibliography 94
8 Internuclear Distances from 1H T1
Relaxation Measurements
in Solution 97
8.1 X−H Distances: Metal–Hydride
Bond Lengths 98
8.1.1 How to Determine Metal–Hydride Bond Lengths
by Standard 1H T1 Measurements 101
8.1.2 Metal–Hydride Bond Lengths by 1H T1sel
and 1H T1min Measurements 104
8.2 Proton–Proton Distances by Standard
1H T1 Measurements 108
8.3 H−H Distances by T1sel/T1bis Measurements 111
8.4 H...H Distances in Intermediates 115

11 Relaxation of Nuclei Other Than 1H
and 2H and Specific Relaxation
Experiments 155
11.1 Chemical Shift Anisotropies and Nuclear
Quadrupole Coupling Constants from T1 Times
of Heavy Nuclei in Solution 156
11.2 Multinuclear Relaxation Approaches to
Complexation, Association and H-bonding 159
11.3 23Na Relaxation in Solutions of Complex
Molecular Systems 162
11.4 Character of Molecular Motions from 17O and 2H
T1 Relaxation in Solution 165
11.5 Two-dimensional T1 and T1ρ NMR Experiments 166
11.6 Chemical Exchange in Complex Molecular
Systems from 15N Relaxation in Solution 168
11.7 R1/R2 Method 170
11.8 Cross-correlation Relaxation Rates
and Structures of Complex Molecular
Systems in Solution 172
11.9 Variable-field Relaxation Experiments 174
Bibliography 176
12 Paramagnetic NMR Relaxation 179
12.1 Theoretical Basis of Paramagnetic Relaxation
Enhancement 179
12.2 Paramagnetic Relaxation Rate Enhancements
in the Presence of Chemical Exchange 185
12.3 Structural Applications of Paramagnetic
Relaxation Rate Enhancement 187
12.4 Kinetics of Ligand Exchange via Paramagnetic
Relaxation Rate Enhancement 191
12.5 Longitudinal Electron Relaxation Time
at Paramagnetic Centers from
Variable-high-field NMR Experiments 193
Bibliography 195

化学家实用NMR驰豫
Practical NMR relaxation for chemists
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