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【求助】国外大学的NMR题

  • ruimingyu11
    2011/01/25
  • 私聊

核磁共振技术(NMR)

  • 国外的NMR题,请高手解答
    1、It is NOT recommended to use a lock solvent when running a 31P spectrum. a.True b. False

    2. In the statements listed below, choose all the correct ones.Choose at least one answer.

    a. zg will 'zero' the memory buffer before starting acquisition.

    b. zg will do 'DS' dummy scans followed by 'NS' actual scans.

    c. zg will always perform multples of 4 scans.

    d. zg will automatically change the temperature of sample to 298 K

    3. The digits shown on the tune card of broad band probeheads should be chosen exactly to get the best tuning and
    matching condition, no matter what sample you use.
    a.True b. False

    4. What is the command you enter to shim the FID on the fly ?Choose one answer. a. go b. zd c. ze d. gs

    5. Let us say, for a total number of NS scans in a 13C experiment, I get a signal to noise ratio (i.e. S/N ) of a peak to
    be 5. I f I want to increase that peak's S/N value to 10, what are the options I have ?

    a. Increase the number of scans NS by a factor of 4 b. Increase the molar concentration of sample by a factor of 2

    c. Nothing can be done d. Increase the receiver gain by a factor of 2


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  • avance

    第1楼2011/01/29

    仅供参考,欢迎指正
    1B大概意思是在测磷谱时不推荐使用氘代溶剂
    2B,执行ZG命令后一半都是先运行DS(dummy scan空扫)然后再starting acquisition。
    3A大概是调谐的问题,不管什么样品都要做调谐,才可以得到最佳状态
    4不知道感觉选项既有布鲁克的命令,也有瓦里安的。
    5A大概是说怎样增加信噪比,只能是增加扫描次数,或者添加更多样品量

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  • lwscut

    第2楼2011/03/04

    1、B
    2、A AND B
    3、B
    4:选D
    5、A

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