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[仪器手册] NMR User Manual-Bruker Avance DPX400 仪器手册zt

瓢虫

2006/07/21

核磁共振技术（NMR）

转载自小木虫，作者：crisoo

Bruker Avance DPX400 仪器手册

供初学者熟悉用

CONTENTS
1 INTRODUCTION................................................................................2
2 NMR FACILITY POLICIES...................................................................6
3 PREPARING FOR ACQUISITION.......................................................7
4 LEAVING THE SPECTROMETER..................................................10
1D EXPERIMENTS..........................................................................11
5 1H NMR........................................................................................12
6 13C NMR.......................................................................15
7 DEPT 45, DEPT 90, and DEPT 135..............................................18
8 DPFGSE-COSY...................................................21
9 DPFGSE-TOCSY.............................................................24
10 DPFGSE-NOE and DPFGSE-ROE...............................................27
11 DPFGSE............................................................................31
12 gs-SELINCOR.......................................................................34
13 19F NMR.........................................................................37
14 31P NMR.............................................................................40
2D EXPERIMENTS.............................................................43
15 gs-COSY.....................................................................44
16 gs-DQF-COSY.......................................................................47
17 TOCSY......................................................................51
18 NOESY and gs-NOESY..............................................55
19 ROESY and T-ROESY...........................................60
20 gs-HMQC.....................................................64
21 gs-HSQC.............................................................................67
22 gs-HMBC............................................................................71
23 CIGAR-HMBC................................................................74
APPENDIXES........................................................................78
APPENDIX A: CLEANING PROCEDURES FOR NMR SAMPLE TUBES...............79
APPENDIX B: MANUAL PHASE CORRECTION OF THE 1D SPECTRUM.........................81
APPENDIX C: MANIPULATING THE 1D SPECTRUM ON THE SCREEN..........................82
APPENDIX D: MANIPULATING THE 2D SPECTRUM ON THE SCREEN....................84
APPENDIX E: ADVANCED PROCESSING OF 2D SPECTRA.............................85
APPENDIX F: ABOUT NOE EXPERIMENTS........................................87
APPENDIX G: TUNING AND MATCHING THE PROBE................................89
APPENDIX H: SOME USEFUL TIPS AND COMMANDS..............................93
APPENDIX I: VARIABLE TEMPERATURE EXPERIMENTS...........................97

Bruker Avance DPX400 仪器手册

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Bruker Avance DPX400 仪器手册

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