谁知道哪有磷谱的化学位移表，特别是固相磷谱的，谢谢大家了

查文献，其中有些文献对特定体系会做总结
计算

P固体核磁的出峰位置比较多，一般在-30～0之间都有位移，同和P相结合的其它元素有关，依照具体情况而定

80ppm到-65ppm之间的偶见过
别的没做过

31P Chemical Shifts
Phosphorous (III) Chemical Shift Table (from Bruker Almanac 1991)
Compound Chemical Shift (ppm)
Relative to 85% H3PO4
PMe3 -62
PEt3 -20
PPr(n)3 -33
PPr(i)3 +19.4
PBu(n)3 -32.5
PBu(i)3 -45.3
PBu(s)3 +7.9
PBu(t)3 +63
PMeF2 245
PMeH2 -163.5
PMeCl2 +192
PMeBr2 +184
PMe2F +186
PMe2H -99
PMe2Cl -96.5
PMe2Br -90.5
Phosphorous (V) Chemical Shift Table (from Bruker Almanac 1991)
Compound Chemical Shift (ppm)
Relative to 85% H3PO4
Me3PO +36.2
Et3PO +48.3
[Me4P]+1 +24.4
[PO4]-3 +6.0
PF5 -80.3
PCl5 -80
MePF4 -29.9
Me3PF2 -158
Me3PS +59.1
Et3PS +54.5
[Et4p]+1 +40.1
[PS4]-3 +87
[PF6]-1 -145
[PCl4]+1 +86
[PCl6]-1 -295
Me2PF3 +8.0

Selective phosphorus regeneration of sinking marine particles: Evidence from 31P-NMR
http://pangea.stanford.edu/research/paytanlab/projects/31PNMR.htm

Solid-state 31P NMR of nucleotide binding proteins
http://www.opus-bayern.de/uni-regensburg/volltexte/2004/443/

Solid-state magic-angle spinning 31P-NMR studies of native casein micelles
http://content.febsjournal.org/cgi/content/abstract/230/2/454

Structural and Solid-State 31P N.M.R. Studies on a Novel Fluorotris(triphenyl-phosphine)copper(I) Adduct


http://www.publish.csiro.au/paper/CH9910427.htm

Application of Spin Counting to the Solid-State 31P NMR Analysis of Pasture Soils with Varying Phosphorus Content
http://soil.scijournals.org/cgi/content/abstract/69/6/2058