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求助大神,177.2450中MDI和TMA的测试方法在哪能找到

食品接触材料

  • (3) The polyamide-imide resins identified in paragraph (a)(1) of this section are heat cured at 600 °F for 15 minutes when prepared for extraction tests and the residual monomers: p,p-diphenylmethane diisocyanate should not be present at greater than 100 parts per million and trimellitic anhydride should not be present at greater than 500 parts per million. Residual monomers are determined by gas chromatography (the gas chromatography method titled “Amide-Imide Polymer Analysis—Analysis of Monomer Content,” is incorporated by reference in accordance with 5 U.S.C. 552(a). Copies are available from the Center for Food Safety and Applied Nutrition (HFS-200), Food and Drug Administration, 5001 Campus Dr., College Park, MD 20740, or available for inspection at the National Archives and Records Administration (NARA). For information on the availability of this material at NARA, call 202-741-6030, or go to: http://www.archives.gov/federal_register/code_of_federal_regulations/ibr_locations.html.).
    这是对MDI和TMA的剩余单体量要求描述,但是却没有提测试方法。FDA这块了解的不多,这个具体的测试方法我要到哪里才能找到呢?主要是前处理的方法。
  • 该帖子已被版主-戎马一生为家国加5积分,加2经验;加分理由:鼓励发帖
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  • m3302418

    第1楼2017/10/16

    只能自问自答了,FDA回复的方法见附件,应该是要用GC的吹扫捕集,还要衍生。

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  • 该帖子已被版主-戎马一生为家国加5积分,加2经验;加分理由:感谢分享
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