电热熔融设备

仪器简介：X射线荧光分析对于粉末样品，目前采用直接压片法制备试样较为普遍，但由于粒度、矿物、偏析等效应的影响，势必带来分析误差，降低元素分析的精密度与准确度，样品制备已经成为一个主要的误差因素。玻璃熔融法制成的试样能消除试样的粒度、矿物、偏析等效应，同时也可降低样品元素间的吸收和增强效应，会明显提高分析的精度和准确度。对于ICP、AA和湿法化学分析手段，对于难溶样品，熔融方法同样是一种非常完美的制样手段。 多年来国内所采用的熔融设备均依赖进口，价格非常昂贵，针对这种局面，本公司科研人员于2002年开发完成了填补国内空白的DY501型电热熔融设备。它吸取了当今国际市场上同类制样设备的优点，其主要性能达到甚至超过国外同类产品。由于其优异的性能和合理的价格，定将取代进口产品，并使原来由于经济原因暂不用熔融设备的用户也能使用它。DY501型电热熔融设备的推出，定将迅速普及熔融制样法，从而提高我国分析界制样的水平，为各行各业带来巨大的经济效益。 Currently, powdered samples for X-ray fluorescence analysis are usually directly pressed into sample pieces. But that kind of sampling has become a major error factor impacting the precision and accuracy of the element analysis due to the granularity effect, mineral effect and segregation effect of the sample pieces. The bead fusion method can eliminate the granularity, mineral and segregation effects of the samples, and can reduce the absorption and enhancement effects between the elements in the sample, and hence evidently increase the precision and accuracy of the analysis. This bead fusion method is a perfect sampling method for ICP, AA, as well as for indissolvable samples in wet chemical analysis. For many years, the fusion machine used in China were all imported from abroad at very high price. To fill up that gap in Chinese science and technology, the research and development personnel in our company developed the DY501 Electroheat Fusion Machine in the year 2002. This fusion machine absorbed the advantages of all the fusion machine of the same kind in the international markets, with key properties up to or even better than those of the overseas products. With its excellent performance and reasonable price, it will take the place of the imported products and can be affordable for the users which are currently not using fusion units just because of economic reasons. The popularization of the DY501 Electroheat Fusion Machine will rapidly promote the bead fusion method in China and hence improve the sampling quality of the element analysis, which can bring tremendous economic benefit for every industry or trade. 公 司 简 介 INTRODUCTION 上海宇索电子科技有限公司是由长期致力于X荧光分析仪销售服务和研究开发的技术人员合资成立的一家高科技企业。公司的创办者在长期的X荧光分析仪的销售服务和研究开发中深切地体会到样品制备对荧光分析的重要性，而最好的样品制备方法就是玻璃熔融法，但当时国内所采用的熔融设备均依赖进口，价格又非常昂贵，所以成立了本公司。 本公司在2002年成立后的短短一年时间里，就开发完成了填补国内空白的DY501型电热熔融设备。至2005年，DY501型电热熔融设备的用户已达近百家，并受到用户的一致好评。公司现有科技人员多名，其中高级工程师3名，博士1名，现正研究开发DY511型全自动电热熔融设备和DY521型全自动单头实验室用小型电热熔融设备，并将于2006年中推向市场。 本公司是样品熔融的专家，分析的好帮手。 Shanghai Yusuo Electronic S&T Co. Ltd. is a high technology enterprise established by the experienced people who focus on the sales, service and research of X-Ray analysis instrument many years. As the bead fusion is widely recognized as valuable means in X-Ray analysis, which can improve the reliability of the analysis results, but in China all the fusion machine has to imported, which very expensive and response time of service is very long. To provide local China solution, Shanghai Yusuo Electronic S&T Co., Ltd was setup on 2002. One year after the 2002, the company introduced DY501 electroheat fusion machine. Till now, there are around hundred systems using in China, which make DY501 a very popular fusion machine. Now the company has many technical developing persons, three of them are senior engineers and one doctor. Now the new model DY511 fully automatic electroheat fusion machine and DY521 fully automatic mini electroheat fusion machine is under developing, and will introduce in the mid of 2006. Yusuo, the expert on bead fusion, your assistant on analysis. 部分用户名单 常州中天钢铁(2台) 苏钢集团公司 紫金矿业股份公司 江苏沙钢集团公司(2台) 内蒙古霍煤鸿骏铝电公司 郑州轻金属研究院 南京梅山矿冶有限公司 天津钢厂(4台) 武汉理工大学 贵阳地球化学研究所 柳州钢铁股份有限公司 湘潭钢铁集团有限责任公司(3台) 江西景德镇陶瓷学院 广东省环境保护监测站 湛江出入境检验检疫局 广东省韶钢集团有限责任公司(2台) 中国科学上海硅酸盐研究所 合肥中皖化学试剂有限公司 泰山玻璃纤维股份有限公司 贵州六盘水市水钢新建炼纲工程 福建省三明市钢厂(2台) 华南理工大学分析测试中心 浙江省师范大学旅游学院 安徽省铜都铜业股份公司金昌冶炼厂 中国科学院西安地球环境研究所 安徽皖维高新材料股份有限公司水泥分公司 技术参数：加热单元：3根双螺旋单端硅碳棒； 最大温度：1250℃，连续可调； 测温单元：2根铂铑热电偶，最高测温1600℃； 容量：同时熔融4个样品（可根据用户要求增加到6个）； 功率：6kw 电源：380-415V,50-60Hz，三相 尺寸（高´ 宽´ 深）：500mm´ 1217mm´ 500mm 重量：115kg. Heating unit: 3 pieces of double helix ,single-end, silicon carbide rod Maximum Temperature: 1250℃,continuously adjustable Temperature measurement unit: 2 pieces of platinum-rhodium thermocouple, with maximum measurable temperature 1600℃ Capacity: 4 samples simultaneously (maximum 6 samples if required by user) Wattage: 6kw Power supply: 380-415V,50-60Hz，three phase Dimension(Height x Width x Depth): 500mm´ 1217mm´ 500mm Weight: 115kg主要特点：◆采用CPU微机及PID控制技术，大屏幕中文显示,菜单式操作； ◆双螺旋硅碳棒加热，铂铑热电偶测温； ◆最多可同时熔融4个样品（可根据用户要求增加到6个）； ◆可预先自由设定最多达10个加热制样程序，其加热过程，升温速度，最终温度，坩埚架摇摆时间、幅度、速度，冷却时间，是否用风扇，风量大小等均可预先设定； ◆除熔融样注入成型模具采用手动外，其他均自动控制，保证了样品的一致性和均匀性，真正做到不同样品仅是其成分不同而没有其他不同； ◆坩埚及成型模具的支架采用耐高温合金钢制成,保证在高温状态下无任何化学反应； ◆熔样室盖打开装置采用链轮杠杆结构，操作轻松自如； ◆具有最低启动温度报警，打开熔样室断电保护； ◆具有过流、过温断电保护并报警，并且过温断电保护采用与加热制样独立的热电偶测温，与加热控制电路一起组成三重保护，使过温断电保护更可靠。 Applies CPU microprocessor and PID control technique, large screen Chinese display, and menu operation Heating with double helix silicon carbide rod temperature measured with platinum-rhodium thermocouple Up to 4 samples can be fused simultaneously (maximum 6 samples if required by user) Up to 10 customized heating programs can be preset within the programs, the heating process, the temperature increase speed, the final temperature, the shaking time, shaking amplitude, and shaking speed of the crucible stool, the cooling time, whether to use fans, the air flow, and so on, all can be preset. Automatic control in all the process except for the filling of the fusion sample, enabling the sameness and homogeneity of the sample all samples are uniformly the same except for the differences in composition The bracket of the crucible and the mould are made of high temperature alloy, which guarantees no chemical reaction in high temperature Chain wheel lever structure is used in the opening device of the cover of the fusion room, trouble-free for user operation With minimum start temperature alarm and power switch-off protection when the cover of the fusion room is open Automatically switching off power and setting alarm for overcurrent and overheat independent temperature measurement thermocouples are used for overheat protection and heating control together with the heating control circuit, they can form treble protection of the system and can make the power switch-off protection for overheat more reliable.

仪器简介：◆可4个样同时熔融，自动摇摆，自动控制； ◆成型模具自动加热，自动冷却，自动成型； ◆大屏幕中文显示，过流过温自动报警切断； ◆可自由设定加温过程，预存多个加温程序。 X射线荧光分析对于粉末样品，目前采用直接压片法制备试样较为普遍，但由于粒度、矿物、偏析等效应的影响，势必带来分析误差，降低元素分析的精密度与准确度，样品制备已经成为一个主要的误差因素。玻璃熔融法制成的试样能消除试样的粒度、矿物、偏析等效应，同时也可降低样品元素间的吸收和增强效应，会明显提高分析的精度和准确度。对于ICP、AA和湿法化学分析手段，对于难溶样品，熔融方法同样是一种非常完美的制样手段。 多年来国内所采用的熔融设备均依赖进口，价格非常昂贵，针对这种局面，本公司科研人员于2002年开发完成了填补国内空白的DY501型电热熔融设备。它吸取了当今国际市场上同类制样设备的优点，其主要性能达到甚至超过国外同类产品。由于其优异的性能和合理的价格，定将取代进口产品，并使原来由于经济原因暂不用熔融设备的用户也能使用它。DY501型电热熔融设备的推出，定将迅速普及熔融制样法，从而提高我国分析界制样的水平，为各行各业带来巨大的经济效益。 Four samples fused simultaneously, with auto-shaking and auto control Auto control means the melting, shaking and standing steps are all precisely repeatable Large screen display auto-alarm and automatic power switching off for overcurrent and overheat Customizable heating process, with several heating programs preset Currently, powdered samples for X-ray fluorescence analysis are usually directly pressed into sample pieces. But that kind of sampling has become a major error factor impacting the precision and accuracy of the element analysis due to the granularity effect, mineral effect and segregation effect of the sample pieces. The bead fusion method can eliminate the granularity, mineral and segregation effects of the samples, and can reduce the absorption and enhancement effects between the elements in the sample, and hence evidently increase the precision and accuracy of the analysis. This bead fusion method is a perfect sampling method for ICP, AA, as well as for indissolvable samples in wet chemical analysis. For many years, the fusion machine used in China were all imported from abroad at very high price. To fill up that gap in Chinese science and technology, the research and development personnel in our company developed the DY501 Electroheat Fusion Machine in the year 2002. This fusion machine absorbed the advantages of all the fusion machine of the same kind in the international markets, with key properties up to or even better than those of the overseas products. With its excellent performance and reasonable price, it will take the place of the imported products and can be affordable for the users which are currently not using fusion units just because of economic reasons. The popularization of the DY501 Electroheat Fusion Machine will rapidly promote the bead fusion method in China and hence improve the sampling quality of the element analysis, which can bring tremendous economic benefit for every industry or trade.技术参数：加热单元：3根双螺旋单端硅碳棒； 最大温度：1250℃，连续可调； 测温单元：2根铂铑热电偶，最高测温1600℃； 容量：同时熔融4个样品（可根据用户要求增加到6个）； 功率：6kw 电源：380-415V,50-60Hz，三相 尺寸（高× 宽× 深）：500mm× 1217mm× 500mm 重量：115kg. Heating unit: 3 pieces of double helix ,single-end, silicon carbide rod Maximum Temperature: 1250℃,continuously adjustable Temperature measurement unit: 2 pieces of platinum-rhodium thermocouple, with maximum measurable temperature 1600℃ Capacity: 4 samples simultaneously (maximum 6 samples if required by user) Wattage: 6kw Power supply: 380-415V,50-60Hz，three phase Dimension(Height × Width × Depth): 500mm× 1217mm× 500mm Weight: 115kg主要特点：◆采用CPU微机及PID控制技术，大屏幕中文显示,菜单式操作； ◆双螺旋硅碳棒加热，铂铑热电偶测温； ◆最多可同时熔融4个样品（可根据用户要求增加到6个）； ◆可预先自由设定最多达10个加热制样程序，其加热过程，升温速度，最终温度，坩埚架摇摆时间、幅度、速度，冷却时间，是否用风扇，风量大小等均可预先设定； ◆除熔融样注入成型模具采用手动外，其他均自动控制，保证了样品的一致性和均匀性，真正做到不同样品仅是其成分不同而没有其他不同； ◆坩埚及成型模具的支架采用耐高温合金钢制成,保证在高温状态下无任何化学反应； ◆熔样室盖打开装置采用链轮杠杆结构，操作轻松自如； ◆具有最低启动温度报警，打开熔样室断电保护； ◆具有过流、过温断电保护并报警，并且过温断电保护采用与加热制样独立的热电偶测温，与加热控制电路一起组成三重保护，使过温断电保护更可靠。 Applies CPU microprocessor and PID control technique, large screen Chinese display, and menu operation Heating with double helix silicon carbide rod temperature measured with platinum-rhodium thermocouple Up to 4 samples can be fused simultaneously (maximum 6 samples if required by user) Up to 10 customized heating programs can be preset within the programs, the heating process, the temperature increase speed, the final temperature, the shaking time, shaking amplitude, and shaking speed of the crucible stool, the cooling time, whether to use fans, the air flow, and so on, all can be preset. Automatic control in all the process except for the filling of the fusion sample, enabling the sameness and homogeneity of the sample all samples are uniformly the same except for the differences in composition The bracket of the crucible and the mould are made of high temperature alloy, which guarantees no chemical reaction in high temperature Chain wheel lever structure is used in the opening device of the cover of the fusion room, trouble-free for user operation With minimum start temperature alarm and power switch-off protection when the cover of the fusion room is open Automatically switching off power and setting alarm for overcurrent and overheat independent temperature measurement thermocouples are used for overheat protection and heating control together with the heating control circuit, they can form treble protection of the system and can make the power switch-off protection for overheat more reliable.

瑞绅葆FMC-01硅钼棒加热熔融炉是瑞绅葆分析技术（上海）有限公司研制的一款XRF分析用玻璃熔片法制样设备。采用玻璃熔片法制得的样品，有效降低甚至消除了样品在XRF分析时遇到的基体效应、颗粒效应和矿物效应等不利因素，极好提高了XRF分析的精确度。在钢铁、冶金、化工、地质、水泥等行业，玻璃熔片法制样有极其广泛的应用。瑞绅葆FMC-01硅钼棒加热熔融炉正是为此而设计的全自动熔样制样设备，整机设计结构合理，采用加热炉体和控制部件分体设计，用户操作简单，人工干预少，只需上样，通过触摸屏设定好熔样程序，熔样过程一键自动完成，熔样过程中设计有用户可调自动摇摆系统保障了熔片的均匀性。瑞绅葆FMC-01硅钼棒加热熔融炉采用硅钼棒加热方式，热电偶实时测温，PID恒温调节，PLC智能控制，整机在控温、稳定性、可操作性等性能上表现优异，加热最高温度可高达1800℃，对不同样品材质有较好的温度适用性，最后制得的样片均匀，质量好，能满足不同行业客户对XRF分析熔样制样需求。优点应用先进的设计理念，采用加热炉体和控制部件分体台式结构设计，整机组合布局合理，体积小，结构外形美观大方。选用高质量硅钼棒加热元件，加热最高温度可达1800℃，抗氧化，耐腐蚀，寿命长。加热炉室内衬选用优质耐火保温材料，确保加热室电热的高效利用及温度稳定性。热电偶实时测温，PID恒温调节，PLC智能控制，保障制样过程精确控制，制片质量优越。全触摸屏显示操作，人机界面友好，人工干预少，只需上样，通过触摸屏设定好熔样曲线，熔样过程一键自动完成。设计有用户可调自动摇摆系统保障了熔片的均匀性和熔片质量，全自动倒模及抖动辅助，适应不同材质样品的制样需要。仪器设计有多重保护（超温、摇摆运动限位保护等），使仪器更安全稳定可靠运行。倒样浇铸在炉内完成，对人体热辐射少，设计有强制风冷系统加快熔片冷却，提高效率。整机升温快、控温精确（±1℃）、节能、运行稳定，工作温度可达1800℃，对不同样品材质有较好的温度适用性，最后制得的样片均匀，较好满足XRF分析。单次可同时熔融四个样片（用户还可定制6个样位机型），整机性价比高。。技术参数型号FMC-01温度范围室温-1800℃升温速度最大45℃/min（熔融加热阶段）加热方式硅钼棒加热控温精度±0.1℃（双热电偶测温）额定功率和电流7.5kW，45A电源单相220V、50/60Hz，保护接地坩埚架摇摆角度最大±75°（分6个级别）坩埚架摇摆频率最大1Hz（分6个等级可选）成型方式自动倒模浇注成型，冷却气流大小，磁搅拌速度可调控制系统集操作显示控制一体真彩液晶触摸屏、PLC控制、PID恒温调节熔样曲线工作模式及各阶段时间预热→氧化→熔融1→熔融2，各阶段时间可调坩埚倒模前静置时间可调坩埚倒模后静置时间可调旋转摆动时间可调熔样工作方式自动进样→熔融摆动→自动倒模→自动出样熔样位4个（可根据用户要求定制6个样位）熔样速度4个/12~18分钟（根据样品的复杂程度而定）设备安全保护断偶、断棒保护、过热保护、运动限位保护。坩埚要求铂黄坩埚（Pt/Au: 95/5），需单独定制仪器重量150kg（主机+控制器）主机和控制器尺寸（L×W×H mm）主机：680×650×560控制器：630×260×420应用领域钢铁、冶金、化工、地质、水泥、陶瓷耐火材料等行业，用于矿石、岩石、土壤、耐火材料、冶金原料等样品的XRF分析——玻璃熔片制样。