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【求助】求助!!!Delta Plus XP的离子源清洗方法!

同位素及其它无机质谱

  • 哪位大侠自己清洗过离子源,或者有清洗方法的,传上来分享一下吧。特别是关于拆装注意等细节,在此先谢谢了!
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  • 52118341

    第1楼2008/04/01

    我也想知道,哪位好心人给点儿建议,手册上讲的太简单了。

    easy-1981 发表:哪位大侠自己清洗过离子源,或者有清洗方法的,传上来分享一下吧。特别是关于拆装注意等细节,在此先谢谢了!

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  • qibiao2008

    第2楼2008/04/18

    8.6.4 CLEANING THE ION SOURCE PARTS
    8.6.4.1 CLEANING THE METALLIC PARTS
    1. Grind all contaminated and discolored metal parts with aluminum oxide powder
    (600 grain). The mechanical cleaning described above must be followed by a chemical
    cleaning.
    2. All parts must be cleaned within a grease dissolving cyclohexane bath. An ultra sonic bath
    will improve and accelerate the cleaning procedure.
    NOTE: Do not use ultrasonic when cleaning the ion source magnets.
    3. Afterwards all parts made of stainless steel should be cleaned in a 3% RBS 50 solution at
    60 °C for about 1 or 2 hours.
    4. After cleaning in RBS 50 and in distilled water, the parts should be dried chemically within
    a Freon bath or a pure alcohol.
    5. After chemical drying, the parts should be additionally dried by a fan or a drying oven to
    eliminate solvent residuals.
    8.6.4.2 CLEANING THE CERAMIC INSULATORS
    1. Use a clean diamond file for eliminating metal abrasion and evaporated films. Use this
    method only for cleaning the ceramic insulator of the cathode and the electron collector.
    2. Anneal the ceramic spacer rings to red heat. Use a propane-oxygen flame or a muffle furnace
    for annealing (maximum temperature: 800-1000 °C).
    Fig. 8.3 Ion Source (Part No.: 111 9440)

    Source Feedthrough, see fig. 8.4
    Source Wiring, see fig. 8.5



    Pos. 26/26a are not shown



    NOTE: The parts marked with an asterisk (*) frequently break. It is recommended
    to provide for replacements before the source is opened.









    Fig. 8.4 Source Feedthroughs




    Fig. 8.4 a Connection Scheme for Lamps
    For part numbers, see page 8 – 46.











    Fig. 8.5 Source Wiring

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  • 戈壁明珠

    第3楼2008/11/17

    应助达人

    您先给仪器的离子源拍个照片,这样就不会装错了。
    拆卸的时候有说明书,按照说明书一个一个部件慢慢拆,搞不清就先拍个照再卸。最后把说明书上要求的需要清洗或打磨的部件做清洗并打磨。然后在组装。后卸的先装。记住所有的线的连接不要弄错。

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