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请问有没有多维(三、四维)NMR在聚合物方面应用的文献??

核磁共振技术(NMR)

  • 如题 有没有多维(三、四维)NMR在聚合物方面应用的文献呢??
    我没有找到,郁闷!
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  • xiaoben412

    第1楼2006/01/04

    好像在03年的macromolecules中有一篇,是杜邦公司研究人员的文章

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  • chprince

    第2楼2006/01/04

    wo我觉得比较少,面太窄了

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  • celan

    第3楼2006/01/05

    这方面的文献很多的,下面给出一些供参考.

    "Characterization of Polymer Chain Ends of Polybutadiene Using 1H/13C/119 Sn Triple Resonance 3D-NMR," Liu, W.; Saito, T.; Li, L.; Rinaldi, P.L.; Hirst, R.; Halasa, A.F.; and Visintainer, J., Macromolecules, 2000, 33, 2364.

    "1H/13C/119Sn Triple Resonance 3D-NMR of Tin-Containing Polybutadiene," Liu, W.; Halasa, A.F.; Visintainer, J.; Hirst, R.; and Rinaldi, P.L., Polymer Preprints, 2000, 41(1), 26.

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  • celan

    第4楼2006/01/05

    NMR 3D Analysis Photopolymerization

    by N. Fatkullin et al
    This volume presents critical reviews of the present and future trends in polymer and biopolymer science including chemistry, physical chemistry, physics and materials science.

    NMR 3D Analysis Photopolymerization's objective is to outline the basic theories and models of linear polymer chain dynamics and to demonstrate the potential of NMR (nuclear magnetic resonance) techniques for probing the characteristics of molecular motions in such systems. From the methodological point of view, it mainly focuses on field-cycling NMR relaxometry and field-gradient NMR diffusometry, but also makes some references to transverse relaxation and the residual dipolar interaction occuring in entangled polymer systems.

    It is addressed to all scientists at universities and in industry who wish to keep abreast of advances in the topics covered.

    Contents

    Polymer Chain Dynamics and NMR
    Introduction
    NMR Methods
    Modeling of Chain Dynamics and Predictions for NMR Measurands
    Experimental Studies of Bulk Melts, Networks and Concentrated Solutions
    Chain Dynamics in Pores ("Artificial Tubes")

    Emerging Technologies for the 3D Analysis of Polymer Structures
    Introduction
    3D Microscopy
    Digital Image Analysis of 3D Structures
    Time Evolution of Bicontinuous Structure in Spinodal Interface of a Binary Polymer Mixture
    Direct Measurement of Interfacial Curvature Distributions in a Bicontinuous Block Copolymer Nanostructure
    Geometrical Similarity/Difference Between Polymer Blend and Block Copolymer Structures

    Two-Photon Photopolymerization and 3D Lithographic Microfabrication
    Introduction
    General Stereolithography Using Femtosecond Lasers
    Fundamentals of Stereolithography using Two-Photon Photopolymerization
    Advanced Techniques in Two-Photon Micro-Nanofabrication
    Applications
    Future Prognosis
    Author Index
    Subject Index

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  • celan

    第5楼2006/01/05

    The 2D and 3D NMR experiments generate huge data sets, Rinaldi noted. The lab
    has a network with primarily Windows NT, ... "We do a lot of polymer analysis,"
    Rinaldi noted. And while there are small compilations of NMR resonances

    http://www.acdlabs.com/publish/sca.html

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  • celan

    第6楼2006/01/05

    It is a package for computer-assisted assignment of 2D, 3D, and 4D NMR. spectra of
    proteins and nucleic acids, which includes tools for ... Polymer Builder. is used
    to construct models of polymer chains from monomers

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  • celan

    第7楼2006/01/05

    3D Methods. 3.4.1 Homonuclear 3D Experiments. 3.4.2 Assignment-oriented
    Heteronuclear 3D NMR. 3.4.3 Heteronuclear 3D with 15N/13C-labeled ... 10.4 Polymer
    Segment End-Structure Determination by Long-Range Correlation Experiments

    Two-Dimensional NMR Spectroscopy: Applications for Chemists and Biochemists, Second Edition, Fully Updated and Expanded to Include Multidimensional Work
    W. R. Croasmun (Editor), Robert M. K. Carlson (Editor)
    ISBN: 0-471-18593-0
    Hardcover
    980 pages
    August 1994

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  • hchy

    第8楼2006/01/05

    谢谢celan老师 真不少啊 我忘了用google搜了,输入Multidimensional和polymer 唰一下就一千多条 真有的忙了

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  • hchy

    第9楼2006/01/06

    其实我想找一些固体核磁多维(三、四维)谱在固态高聚物方面的应用,还是比较困难啊,现在找到的大多是用液体多维NMR研究聚合物

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  • someoney

    第10楼2006/01/07

    学到了好多东西啊

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