仪器信息网APP
选仪器、听讲座、看资讯
当前位置: 仪器社区 >质谱 > ICP-MS > 帖子详情

新手求教

ICP-MS

  • 进入ICP-MS样品中含10%或更高的硝酸,对结果会有什么影响?对仪器会有什么负面影响?
    另外,手册上说样品中总盐的含量要小于0.2%,如果样品中含有20%左右的硝酸氨或其他氨盐(如氯化铵等),还可以得到好的结果吗?

    多谢!
0
    +关注 私聊
  • 第2楼2004/10/14

    应该会很损锥吧
    如果银子多,可以长期试的

    cafu2000 发表:进入ICP-MS样品中含10%或更高的硝酸,对结果会有什么影响?对仪器会有什么负面影响?
    另外,手册上说样品中总盐的含量要小于0.2%,如果样品中含有20%左右的硝酸氨或其他氨盐(如氯化铵等),还可以得到好的结果吗?

    多谢!

0
    +关注 私聊
  • 第3楼2004/10/25

    找到了一个解答:

    Total dissolved solids (TDS)

    The total amount of material (including major species) in solution in your samples. In general this should be between 0.2% and 0.5%. The general rule for maximum dissolved solids is to consider the boiling point of the matrix oxide; if the matrix oxide is refractory the material is more liable to build up on the cones and the maximum TDS should be kept to 0.2%. If the matrix oxide does not form a refractory oxide, then material is less likely to build up on the cones, and the maximum TDS can be 0.5%. If the matrix forms a gaseous oxide such as with high levels of organic material (ammonium acetate, digested biological material etc.), then the level can go as high as 10%. As long as the TDS remains within sensible limits the lenses require cleaning routinely for normal sample loads every 6 - 12 months which is the normal preventative maintainance secheduling, outside of this the user should not need to attend to the lens components of the X Series ICP mass spectrometer.

0
猜你喜欢最新推荐热门推荐更多推荐
举报帖子

执行举报

点赞用户
好友列表
加载中...
正在为您切换请稍后...