方法参数： Sample Inlet : GC Injection Source : Manual Mass Spectrometer : Enabled Oven Equilibration Time 0.5 min Oven Program On 40 癈 for 2 min then 8 癈/min to 120 癈 for 0 min then 8 癈/min to 160 癈 for 5 min Run Time 22 min 1 min (Post Run) 230 癈
Back SS Inlet He Mode Split Heater On 230 癈 Pressure On 11.962 psi Total Flow On 79.5 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 mL/min After 2 min Split Ratio 50 :1 Split Flow 75 mL/min
Thermal Aux 1 {MSD Transfer Line} Heater On Temperature Program On 280 癈 for 0 min Run Time 22 min
Column #1 HP-INNOWax Polyethylene Glyco: 853.70266 HP-INNOWax Polyethylene Glyco 260 癈: 30 m x 250 祄 x 0.25 祄 In: Back SS Inlet He Out: Vacuum
(Initial) 40 癈 Pressure 11.962 psi Flow 1.5 mL/min Average Velocity 44.411 cm/sec Holdup Time 1.1258 min Flow Program On 1.5 mL/min for 0 min Run Time 22 min 1 min (Post Run) 1.5 mL/min
MS ACQUISITION PARAMETERS
General Information ------- -----------
Tune File : atune.u Acquistion Mode : Scan
MS Information -- -----------
Solvent Delay : 6.00 min
EMV Mode : Relative Relative Voltage : 0 Resulting EM Voltage : 906
[Scan Parameters]
Low Mass : 30.0 High Mass : 500.0 Threshold : 0 Sample # : 2 A/D Samples 4 Plot 2 low mass : 30.0 Plot 2 high mass : 500.0
[MSZones]
MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C
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