enhua
第1楼2010/05/05
厦门农产品技术中心与安捷伦合作开展鱼种贝类鉴定研究
Agricultural Technology Center in Xiamen in collaboration with Agilent identification of species of shellfish
http://www.instrument.com.cn/news/20100510/042141.shtml
质检总局09年批准筹建66家国家检测重点实验室
General Administration in 2009 approved the establishment of 66 State Key Laboratory testing
http://www.instrument.com.cn/news/20100318/040113.shtml
2010年01月07日厦门出入境检验检疫系统2009年科学发展工作述评
January 7, 2010 Xiamen Entry-Exit Inspection and Quarantine system work 2009 Review of Scientific Development
http://finance.sina.com.cn/roll/20100107/08543173593.shtml
3 食品检测部分
(1)主要的业务内容:食品、动植物及其产品的微生物检验,农药残留量、兽药残留量、重金属、毒素等有毒有害物质检验和食品添加剂检验,食品的毒理学检验,转基因产品的检测以及动植物传染病、寄生虫病、病虫、杂草等有害生物的检疫,食品容器及食品包装材料安全卫生检验。
(2)承检实验室:技术中心承担食品、食品容器、食品包装材料、动植物及其产品检测的实验室:食品理化实验室、微生物实验室、植物检疫实验室、动物检验检疫实验室、化矿金化学实验室。
(3)实验室检测业绩:2006~2009年承检上述工作的情况大致如下:
①涉及的种类:饼干糕点,糖及糖果,酒,饮料,调味品,罐头食品,蔬菜,真菌蘑茹类,粮食、植物淀粉及制品,水产品,动物肉及制品,食品添加剂,乳与乳制品,动植物油脂,蛋及蛋制品,以及食品用容器(陶瓷类,塑料类,金属类、纸制品类和竹木制品类等)和食品包装材料等,共约300多个品种。
②主要检验的项目:食品化学项目(重金属,农药残留,兽药残留,毒素等有害物质,食品添加剂以及其它一些常规化学分析项目)约123553项次;微生物检验项目(细菌总数、大肠杆菌、各种致病菌和转基因产品检测)约25668项次;动植物检疫检验项次约26858项次。
(4)主要的分析和检测设备:液相串联质谱仪(LC-MS-MS, 3台), 液相飞行时间质谱仪(1台),气相色谱仪(GC,多台)、气质联用仪(GC-MS,多台)、高效液相色谱仪(HPLC,多台,美国安捷伦公司,美国PE公司)、原子吸收分光光度计(AAS,2台)、原子荧光分光光度计(AFS)、荧光PCR仪(Sequence Detection System (Fluorescence Quantitative PRC System),美国Applied Biosystems公司)、凝胶图像分析系统(Gel Documentation and Analysis System 厂商:英国Uvilec.co.uk)自动微生物检测系统(VITEK AUTOMICROBIC SYSTEM ,厂商:BIO MERIEUX VITEK INC.U.S.A)、酶标仪(Microplate reader 厂商:美国Bio-Rad公司)等各类先进的分析检测仪器60多台。
(5)实验室设施情况:检验用房面积约2000多平方米,设置有专用的微生物、食品化学、转基因、毒理等方面的检验检疫设施。
(6)实验室近年来参加的能力验证情况:近年来共参加食品和动植物产品中农兽残、重金属、微生物、病原菌、转基因等相关领域40次能力验证,结果均为满意,见表1;参加实验室间比对4次,结果均为满意,见表2。
4 技术中心动物源性残留监控
(1)组织结构
技术中心是国家质检总局指定的35个残留监测实验室之一,承担着厦门局辖区内的残留监控样品的检测任务。
技术中心平面效果图Technology Center Graphic renderings
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鸟瞰Bird's eye view
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中心动工前,打地基,右上角,吊塔下的岛为鼓浪屿
Center prior to the commencement upper right corner hit the foundation, under the hanging tower island Gulangyu
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2008年夏天,中心完工。远方背景为厦门岛东渡区域,右上角的岛为鼓浪屿
The summer of 2008, the Center completed. Going the distance the background for the area of Xiamen Island, the upper right corner of the island as Gulangyu
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2008.9.8,厦门九八贸洽会前落成
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中心楼群封顶仪式for blocks of cap ceremony
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办公室,墙刚刚砌好的时候。Office, when the wall just finish
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装修好的办公室A furnished office
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enhua
第2楼2010/05/05
1 Technical Introduction http://www.xmciqtech.gov.cn/Article_Index.asp
Xiamen Inspection & Quarantine Technology Center (hereinafter referred to Technology Center) is a state approved the establishment of an independent cause of registered legal entities, Xiamen Entry-Exit Inspection and Quarantine under. Mainly engaged in mechanical and electrical products, food, agricultural products, plants and animals and their products, products of gold mining, packaging materials, inspection and testing services, etc., as well as research and manufacturing standard, test technology development, technical consulting, training and so on.
Technology Center consists of seven laboratories, a sub-centers and three administrative departments. Electrical Laboratory, respectively (National Electrical Safety testing laboratory), Plant Quarantine Laboratory (National Vegetable Seed and Plant Quarantine Laboratory seed-borne virus), food physics and chemistry laboratory, microbiology laboratory, animal inspection and quarantine laboratory, gold mine of chemical laboratory, metals and packaging laboratories; with the law-abiding center; and business development, general management, finance (see Figure 1 Organization Chart).
现在开始介绍实验室了
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2004年巴西“种衣剂”大豆事件中 ,登轮检查种衣剂大豆,7舱,5万吨,在旧实验楼。
2004 Brazil "Seed" soybean event, board the vessel inspection of soybean seed coating
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旧技术中心实验楼Old Laboratory Building Technology Center
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旧楼实验室照片回忆Memories of old lab photos
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旧楼实验室残留分析试验台Residue analysis laboratory test table of old buildings
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下面开始介绍新楼实验室The following laboratory began on the new floor
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搬家前的走廊Corridor before moving
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气瓶室Cylinder chamber
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气体通过管路送到仪器Gas delivered by pipeline equipment
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样品制备,研磨。细磨;Sample preparation, grinding. Fine grinding;
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粗磨Coarse grinding
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前处理间Pre-treatments
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通风橱aerator
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enhua
第3楼2010/05/05
After several years of construction, technology center already has a solid detection capabilities. Advanced testing equipment and a large analysis of more than 1,000 sets of equipment, worth 100 million yuan, including API5000 LC-MS-MS, liquid time of flight mass spectrometer, triple quadrupole GC-MS, matrix-assisted laser desorption ionization - time of flight mass spectrometry, inductively coupled plasma mass spectrometry, confocal laser scanning microscopy, X-ray fluorescence spectrometer, X-ray diffraction, single-stage quadrupole GC-MS, DNA sequencer, automated microbial identification instrument, Denaturing high liquid chromatography, inductively coupled plasma emission spectrometry, direct-reading spectrometer, Fourier transform infrared spectroscopy, desktop scanning electron microscope, EMI Receivers EMC, EMS radiation immunity tester, rechargeable battery discharge tester HPGe γ spectrometry, liquid chromatography, gas chromatography, atomic absorption spectrometry, atomic fluorescence morphological analyzer, ion chromatograph, thermoluminescence detectors and other international most advanced equipment and 3m wave darkroom, greenhouse plant quarantine viruses and other advanced testing facilities. In addition to first class equipment, the technology center also brings together a highly educated and experienced team of key technical personnel, including 11 PhD in PhD 2, MA 23, senior professional titles, 32 people (including fellow 3 ), intermediate grade 38. Laboratory area of 10 002 more than 1000 square meters, of which an area of 10,000 square meters of new laboratory building was Haicang August 25, 2008 opening. The new laboratory building, experimental environment has been greatly improved laboratory facilities are fully updated, new large-scale purchase of a dozen units have been installed and adjusted and put into use, to further enhance the level of laboratory testing.
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旋转蒸发仪,现在残留分析比较少用,毒理实验项目同事比较常用。Rotary Evaporator,
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固相萃取,手动灵活,好用Solid phase extraction, manual and flexible, easy to use
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恒温振荡Temperature oscillation
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平行蒸发,大体积提取浓缩,好用。Parallel evaporation, mass extraction and concentration, easy to use
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氮吹仪:30ml*5通道*10个口,最常用,液氮供气,便宜。缺点:体积限制。
Nitrogen blowing instrument: 30ml * 5 channels * 10 I, the most commonly used liquid nitrogen gas, cheap. Disadvantages: size limit.
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超临界Supercritical
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超临界SFE,SFE Supercritical
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快速溶剂萃取ASE,Accelerated solvent extraction ASE
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GPC,凝胶渗透
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搬到新楼后增加GPC浓缩装置。
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吉尔森固相萃取Gilson SPE
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enhua
第4楼2010/05/05
Current technology centers as well as Fujian, Xiamen City has become the largest mechanical and electrical products, food, animals and plants and their products, chemical products and packaging materials, gold mining professional testing organization. Holds the latest detection methods, with ISO, GB, JIS, ASTM, IEC, EN, SN, etc. are the latest detection methods. Technology Center of "scientific rigor, fair and accurate, high quality and efficient and dedicated service", in accordance with ISO / IEC 17025 standard to establish, implement and maintain consistent with the scope of laboratory quality management system, standing on third-party impartiality, independence to carry out the entry inspection / testing work, a survey report.
2 Technical Center laboratory has obtained the following qualifications and accreditation - China National Accreditation Board for Conformity Assessment (CNAS), - National Measurement Certification Compliance (CMA) test unit - the State Science Commission finds that the scientific outcome identification of national testing organizations - national identity monitoring Committee approval of GMO testing laboratory - Fujian Province governance "table pollution," Evaluation of quality control indicators for monitoring food safety agency - Japan Ministry of Health registration Korean Food and Drug Administration approved and accredited food testing laboratory - into the designated AQSIQ special export cosmetic testing laboratories - AQSIQ designated testing laboratory mercury content
Food testing part 3
(1) Major Business: food, animals and plants and their products of microbial testing, pesticide residues, veterinary drug residues, heavy metals, toxins and other toxic substances testing and inspection of food additives, food toxicology testing, genetically modified products Detection of animal and plant diseases, parasitic diseases, pests, weeds and other pests of quarantine, food containers and food packaging materials safety and health inspection.
(2) principal inspection laboratory: Technical Center has food, food containers, food packaging materials, animals, plants and product testing laboratories: Food physics and chemistry laboratory, microbiology laboratory, plant quarantine laboratory, animal inspection and quarantine laboratories chemical laboratory of mining gold.
(3) laboratory test results: review 2006 to 2009 bearing the above-mentioned is as follows:
① species involved: biscuit cake, sugar and sweets, alcohol, beverages, condiments, canned food, vegetables, fungi, mushroom type, food, starch and plant products, aquatic products, animal meat and products, food additives, milk and milk products, animal fat, eggs and egg products, and food with a container (ceramic, plastic, metal, paper and wood products category, etc.) and food packaging materials, a total of about 300 species.
- AQSIQ import of specified hazardous substances in the special paint testing laboratories - AQSIQ formaldehyde wood products designated by special testing laboratory - the Kimberley Process rough diamond designated inspection agencies - Electronics Lab 3C Certification - China Quality Certification Centre (CQC) voluntary certification of products authorized by the designated laboratories - Fujian Province People's Court expert
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常规设备General Equipment
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pH计,pH meter
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自动滴定Automatic titration
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高温室Oven
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烘箱
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马弗炉Muffle furnace.
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FOSS,定氮仪FOSS, Nitrogen Determination Apparatus
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FOSS,脂肪测定仪FOSS, fat analyzer
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分光光度计Spectrophotometer
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enhua
第5楼2010/05/05
② major test of the project: Food Chemistry project (heavy metals, pesticides, animal drug residues, toxins and other harmful substances, food additives, and other routine chemical analysis of the project) about 123 553 Ci; microbiological test items (the total number of bacteria, E. coli, the pathogens and GMO detection) is about 25,668 times; animal and plant quarantine inspection of about 26,858 times entry times.
(4) the main analysis and testing equipment: liquid tandem mass spectrometry (LC-MS-MS, 3 units), time of flight mass spectrometry Liquid (1 unit), gas chromatography (gc, more than one), gc meter (gc-MS, multiple), high performance liquid chromatography (HPLC, more than the United States Agilent, U.S. PE firm), atomic absorption spectrophotometer (AAS, 2 sets), atomic fluorescence spectrometry (AFS) fluorescence PCR instrument (Sequence Detection System (Fluorescence Quantitative PRC System), the United States Applied Biosystems Inc.), gel image analysis system (Gel Documentation and Analysis System Manufacturers: British Uvilec.co.uk) automatic microbial detection system (VITEK AUTOMICROBIC SYSTEM, Manufacturers: BIO MERIEUX VITEK INC.USA), microplate reader (Microplate reader manufacturers: the United States Bio-Rad Corporation) and other kinds of advanced testing instruments more than 60.
(5) laboratory facilities: The test covers a floor space of 2,000 square meters, set up a dedicated micro-organisms, food chemistry, transgenic, toxicological aspects of inspection and quarantine facilities.
(6) participate in proficiency testing laboratory in recent years: The years of middle peasants to participate in animal food and animal and plant products residues, heavy metals, microbes, pathogens, genetically modified and other related fields 40 proficiency testing, the results are satisfactory, see Table 1; participate in inter-laboratory comparison 4 times and the results are satisfactory, in Table 2.
4 technical centers residue monitoring of animal origin (1) Structure Technology Center is designated by the State Administration of Quality Supervision 35 one residue monitoring laboratory, undertaking Xiamen Council area of residue monitoring samples detection tasks.
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古老的岛津,填充柱气相色谱。Shimadzu ,years old, packed column gas chromatography
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古老的5890,手动调节The old 5890, manual adjustment
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gc7890,电子流量控制。 有双塔、双FPD方式。gc7890, electronic flow control
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gc顶空装置Headspace gc devices
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氢气发生器Hydrogen Generator
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单四极杆气质,实验室最早的气质。6、7年前的设备条件很差。
Single quadrupole temperament, the earliest laboratory 6,7 years ago, the equipment condition in poor
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Varian 320gcMSMS,效果不错,洗源麻烦。Varian 320gcMSMS, good results, wash the source trouble.
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离子肼气质
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agilent1200,2台,配置不同,常压配置。agilent1200, 2 sets of different configurations
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agilent1200正面照
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waters2695,不错。
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离子色谱,测水质项目Ion chromatography, water quality testing project
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enhua
第6楼2010/05/05
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5楼 液相,液质,气相,气质,一字排开5th Floor, liquid, liquid mass, gas, temperament, lined up
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API3000
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waters UPLC-TQD
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waters UPLC-TOF
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API5000用的氮气发生器API5000 with the nitrogen generator
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API5000的机械泵API5000 mechanical pump
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微波消解Microwave digestion
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原子荧光Atomic Fluorescence
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DOS年代的Varian
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崭新的Varian
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agilent 的ICP-MS
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