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二硫代氨基甲酸酯类农药检测

农残检测

  • 二硫代氨基甲酸酯类农药 与 氯化亚锡反应时,加热温度应该控制在什么温度?能用其他的还原剂吗?
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  • 雾非雾

    第1楼2012/03/29

    应助达人

    详情请参下贴6、7楼
    http://bbs.instrument.com.cn/shtml/20090103/1681211/

    我在故我思(hotdoglet) 发表:2.2 For Mancozeb in Water
    An 8 mL portion of sample was placed into a 40 mL vial along with 10% EDTA, and 3% nCl2/8N HCl solution and capped. The samples were placed in a heating block at 100℃for four hours with shaking at various time intervals. The samples were then analyzed by GC/MSD
    using SIM.

    附件

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