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[求助]请大家看看这种分析粒径分布的方法!

  • superhanlei
    2006/05/24
  • 私聊

透射电镜(TEM)

  • 我在查阅文献时看到有的学者通过TEM和“ellipse-fitting method”来研究纳米颗粒的粒径分布。原文如下:
    Crystal outlines were digitized from scanned,low-magnification TEM photomicrographs and their dimensions estimated by calculating the best fit of an ellipse(of same surface) to the contours. The length (L) and width (W) of a crystal were then matched to the major and minor axes, respectively, of the best-fitting ellipse.
    The sizes are the averages of L and W; the shape factors,describing the elongation of the crystals, were chosen asthe ratio W/L.
    您见过这种分析方法吗?谢谢!
    +关注 私聊
  • 天黑请闭眼

    第1楼2006/05/25

    椭圆吻合近似?就是用一个椭圆形去对,如果吻合的好,就用椭圆的长短轴来定义颗粒的长和宽。
    没有听说过,不过gatan给出的统计结果让我觉得他们可能用的就是这个方法。

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