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ICP-OES检测出的数据中带有uv、x或者ox的是什么意思呢

ICP光谱

  • 如题,需要补充的是,带有x是钙、钾元素,但其rsd正常。请指教!
  • 该帖子已被版主-不忘初心加2积分,加2经验;加分理由:话题
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  • 依风1986

    第1楼2014/01/12

    应助达人

    具体哪一款ICP,我猜楼主应该是安捷伦的(原瓦里安的)这个可以在软件查找代码意思,X就是超出范围,比如你的工作曲线中钙最高点是5mg/L,实际样品钙含量已经超过5mg/L

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  • wccd

    第2楼2014/01/13

    应助达人

    此问题转ICP版讨论更专业一些。

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  • abcpgf

    第3楼2014/01/13

    应助达人

    这个其实在仪器帮助有说明的。

    Error Flags
    Each concentration result may appear with a concentration result 'Flag'. The following table lists each possible concentration result flag and its description. The flags are listed in the order in which they are prioritized, from highest to lowest. If a sample concentration results in more than one error being flagged, the flag with the highest priority is displayed.

    Error flags will be displayed in red text on the Analysis Worksheet. However, if there is more than one flag related to a sample, only the flag of highest priority (as discussed above) will be displayed. To view all of the flags related to a particular sample, highlight the sample and open the Edit Replicates dialog box, which can be accessed from the Edit menu.

    Flag Description
    o Replicate signal overrange
    QC--- QC test failed
    S--- Standard addition failure
    e--- Edited result
    C--- Fitted background error seen on replicates, due to non-convergence
    D ---Fitted background error seen on replicates, unable to be modelled due to insufficient spectral data
    uncal Uncalibrated results
    i--- No internal standard correction applied
    n--- Interference correction not applied (line has a related interferent that was not successfully calculated)
    a ----Solution overrange and automatically diluted
    u--- Under-range (< blank)
    v--- Under valid range (< minimum concentration)
    x---- Extended calibration range (> maximum concentration)
    b---- Line has a related interferent that is above the extended calibration range (IEC correction still applied)

    There are a number of default QC failure flag names, which are listed on the QC Test types and Failure flags page. However, you can change these flag names in the Edit QC Test Definition dialog box.

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  • 守一

    第4楼2014/01/14

    楼上说得很清楚了,OX应该是饱和了

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  • 千层峰

    第5楼2014/01/15

    抽时间看看仪器说明书还是有用的。

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  • 依风1986

    第6楼2014/01/15

    应助达人

    版主,您这直接帮助软件吧!还是翻译下更好

    abcpgf(abcpgf) 发表:这个其实在仪器帮助有说明的。

    Error Flags
    Each concentration result may appear with a concentration result 'Flag'. The following table lists each possible concentration result flag and its description. The flags are listed in the order in which they are prioritized, from highest to lowest. If a sample concentration results in more than one error being flagged, the flag with the highest priority is displayed.

    Error flags will be displayed in red text on the Analysis Worksheet. However, if there is more than one flag related to a sample, only the flag of highest priority (as discussed above) will be displayed. To view all of the flags related to a particular sample, highlight the sample and open the Edit Replicates dialog box, which can be accessed from the Edit menu.

    Flag Description
    o Replicate signal overrange
    QC--- QC test failed
    S--- Standard addition failure
    e--- Edited result
    C--- Fitted background error seen on replicates, due to non-convergence
    D ---Fitted background error seen on replicates, unable to be modelled due to insufficient spectral data
    uncal Uncalibrated results
    i--- No internal standard correction applied
    n--- Interference correction not applied (line has a related interferent that was not successfully calculated)
    a ----Solution overrange and automatically diluted
    u--- Under-range (< blank)
    v--- Under valid range (< minimum concentration)
    x---- Extended calibration range (> maximum concentration)
    b---- Line has a related interferent that is above the extended calibration range (IEC correction still applied)

    There are a number of default QC failure flag names, which are listed on the QC Test types and Failure flags page. However, you can change these flag names in the Edit QC Test Definition dialog box.

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  • junhuahao

    第7楼2014/01/16

    不管哪个牌子的仪器,仪器说明书上都会有介绍的

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  • abcpgf

    第8楼2014/01/16

    应助达人

    你有空就代劳一下吧。

    依风1986(xurunjiao5339) 发表:版主,您这直接帮助软件吧!还是翻译下更好

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  • 依风1986

    第9楼2014/01/16

    应助达人

    那就百度翻译吧!可能专业词语不专业!

    abcpgf(abcpgf) 发表:你有空就代劳一下吧。

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  • abcpgf

    第10楼2014/01/17

    应助达人

    大致意思一致就好。

    依风1986(xurunjiao5339) 发表:那就百度翻译吧!可能专业词语不专业!

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