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EELS光谱收集时特定损失能量选择

透射电镜(TEM)

  • 请问各位,做EELS时一般是在哪里输如特定电子的损失能量?spectrum offset or drift tube or energy shift?
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  • zwhn2001

    第2楼2014/09/04

    一定不要用drift tube,最好用energy shift, 至于原因我还不太清楚。

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  • 大布口袋

    第3楼2014/09/04

    Three ways to shift a spectrum
    1. Magnetic prism – changing prism strength (Energy Shift)
    2. High tension – electron accelerating voltage (Offset)
    3. Drift tube – an extra retarding magnetic field, which responds faster than others, up to 1000eV shift (Drift Tube)

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    1. Spectroscopy: Energy Shift (or Drift Tube) – not to compromise the illumination in STEM
    2. Imaging: Offset – so electrons used to form the filtered image are at the alignment energy while travelling in the imaging system

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  • xdd1987

    第4楼2014/09/04

    非常感谢您的回复

    zwhn2001(zwhn2001) 发表:一定不要用drift tube,最好用energy shift, 至于原因我还不太清楚。

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  • xdd1987

    第5楼2014/09/04

    我看三楼的说不要用drift tube,楼主能帮忙解释一下吗?

    大布口袋(taboo) 发表:Three ways to shift a spectrum
    1. Magnetic prism – changing prism strength (Energy Shift)
    2. High tension – electron accelerating voltage (Offset)
    3. Drift tube – an extra retarding magnetic field, which responds faster than others, up to 1000eV shift (Drift Tube)

    Default
    1. Spectroscopy: Energy Shift (or Drift Tube) – not to compromise the illumination in STEM
    2. Imaging: Offset – so electrons used to form the filtered image are at the alignment energy while travelling in the imaging system

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  • 大布口袋

    第6楼2014/09/05

    哈哈 我不是楼主 楼主帮忙解释下吧

    xdd1987(xdd1987) 发表:我看三楼的说不要用drift tube,楼主能帮忙解释一下吗?

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  • zwhn2001

    第7楼2014/09/06

    I think I got it.

    if the beam is well aligned, when you change the drift tube, you are changing the alignment of the energy filter. This may lead to the loss of some resolution.

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