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加标法定量到底是怎么实现的?

  • 跳跳彩糖
    2018/03/20
  • 私聊

气相色谱(GC)

  • Quantitative Analysis of the Key Aroma Compounds in theRaw and the Heated Soy Sauces by Standard Addition Method.
    An aliquot (5 mL) of the soy sauce with added 2-octanol (4150 μg/L) and the standard solution (0, 100, or 200 μL) containing the chemicals listed in Table 1 was concentrated to about 100 μL using he same concentration method described above. The respective aroma concentrates were analyzed by gc-MS in the synchronous selected ion monitoring and full scan (SIM/scan) mode. On the basis of the relationship between the ratio of the total area count of each key aroma compound to that of 2-octanol and the added concentration of each compound, the quantitative analysis of the key aroma compounds was performed by calculation from the approximated curve using the linear least-squares method. The respective quantitative values of the key aroma compounds were determined by averaging the triplicate experiments。
    文献里是这样描述加标法的,但是后面计算的部分我总也倒腾不过来,在这里请教各位啦!
  • 该帖子已被版主-zyl3367898加2积分,加2经验;加分理由:鼓励发帖
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  • PAEs

    第1楼2018/03/21

    应助达人

    外文啊?看不懂。。。。

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  • xiaogumd11

    第2楼2018/03/21

    应助达人

    你这个加标应该是混标(香气化合物)根据相关标准,应该有怎么进行加标定量的

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