150个基本的NMR实验(PDF文件)和200个NMR实验

Chapter 5 Dynamic NMR Spectroscopy
Exp. 5.1: Low Temperature Calibration with Methanol
Exp. 5.2: High Temperature Calibration with 1,2-Ethanediol
Exp. 5.3: Dynamic 1H NMR Spectroscopy on Dimethylformamide
Exp. 5.4: The Saturation Transfer Experiment
Exp. 5.5: Measurement of the Rotating Frame Relaxation Time T1r
· Chapter 6 1D Multipulse Sequences
Exp. 6.1: Measurement of the Spin-Lattice Relaxation Time T1
Exp. 6.2: Measurement of the Spin-Spin Relaxation Time T2
Exp. 6.3: 13C NMR Spectra with SEFT
Exp. 6.4: 13C NMR Spectra with APT
Exp. 6.5: The Basic INEPT Technique
Exp. 6.6: INEPT+
Exp. 6.7: Refocused INEPT
Exp. 6.8: Reverse INEPT
Exp. 6.9: DEPT-135
Exp. 6.10: Editing 13C NMR Spectra with DEPT
Exp. 6.11: Multiplicity Determination with PENDANT
Exp. 6.12: 1D-INADEQUATE
Exp. 6.13: The BIRD Filter
Exp. 6.14: TANGO
Exp. 6.15: The Heteronuclear Double Quantum Filter
Exp. 6.16: Purging with a Spin-Lock Pulse
Exp. 6.17: Water Suppression by Presaturation
Exp. 6.18: Water Suppression by the Jump and Return Method
· Chapter 7 NMR Spectroscopy with Selective Pulses
Exp. 7.1: Determination of a Shaped 90&; 1H Transmitter Pulse
Exp. 7.2: Determination of a Shaped 90&; 1H Decoupler Pulse
Exp. 7.3: Determination of a Shaped 90&; 13C Decoupler Pulse
Exp. 7.4: Selective Excitation with DANTE
Exp. 7.5: SELCOSY
Exp. 7.6: SELINCOR: Selective Inverse H,C Correlation via 1J(C,H)
Exp. 7.7: SELINQUATE
Exp. 7.8: Selective TOCSY
Exp. 7.9: INAPT
Exp. 7.10: Determination of Long-Range C,H Coupling Constants
Exp. 7.11: SELRESOLV
Exp. 7.12: SERF
· Chapter 8 Auxiliary Reagents, Quantitative Determinations,
and Reaction Mechanisms

Exp. 8.1: Signal Separation Using a Lanthanide Shift Reagent
Exp. 8.2: Signal Separation of Enantiomers Using a Chiral Shift Reagent
Exp. 8.3: Signal Separation of Enantiomers Using a Chiral Solvating Agent
Exp. 8.4: Determination of Enantiomeric Purity with Pirkle's Reagent
Exp. 8.5: Determination of Enantiomeric Purity by 31P NMR
Exp. 8.6: Determination of Absolute Configuration by the Advanced Mosher Method
Exp. 8.7: Aromatic Solvent-Induced Shift (ASIS)
Exp. 8.8: NMR Spectroscopy of OH-Protons and H/D Exchange
Exp. 8.9: Isotope Effects on Chemical Shielding
Exp. 8.10: pKa Determination with 13C NMR
Exp. 8.11: The Relaxation Reagent Cr(acac)3
Exp. 8.12: Determination of Paramagnetic Susceptibility by NMR
Exp. 8.13: 1H and 13C NMR of Paramagnetic Compounds
Exp. 8.14: The CIDNP Effect
Exp. 8.15: Quantitative 1H NMR Spectroscopy: / Determination of the Alcohol Content of Polish Vodka
Exp. 8.16: Quantitative 13C NMR Spectroscopy with Inverse Gated 1H-Decoupling
Exp. 8.17: NMR Using Liquid-Crystal Solvents

Chapter 9 1D Heteronuclear NMR Spectroscopy
Exp. 9.1: 1H-Decoupled 15N NMR Spectra with DEPT
Exp. 9.2: 1H-Coupled 15N NMR Spectra with DEPT
Exp. 9.3: 19F NMR Spectroscopy
Exp. 9.4: 29Si NMR Spectroscopy with DEPT
Exp. 9.5: 29Si NMR Spectroscopy with Spin-Lock Polarization
Exp. 9.6: 119Sn NMR Spectroscopy
Exp. 9.7: 2H NMR Spectroscopy
Exp. 9.8: 11B NMR Spectroscopy
Exp. 9.9: 17O NMR Spectroscopy with RIDE
Exp. 9.10 47/49Ti NMR Spectroscopy with ARING
· Chapter 10 The Second Dimension
Exp. 10.1: 2D J-Resolved 1H NMR Spectroscopy
Exp. 10.2: 2D J-Resolved 13C NMR Spectroscopy
Exp. 10.3: The Basic H,H-COSY Experiment
Exp. 10.4: Long-Range COSY
Exp. 10.5: Phase-Sensitive COSY
Exp. 10.6: Phase-Sensitive COSY-45
Exp. 10.7: E.COSY
Exp. 10.8: Double Quantum Filtered COSY with Presaturation
Exp. 10.9: Fully Coupled C,H Correlation (FUCOUP)
Exp. 10.10: C,H Correlation by Polarization Transfer (HETCOR)
Exp. 10.11: Long-Range C,H Correlation by Polarization Transfer
Exp. 10.12: C,H Correlation via Long-Range Couplings (COLOC)
Exp. 10.13: The Basic HMQC Experiment
Exp. 10.14: Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling
Exp. 10.15: Poor Man's Gradient HMQC
Exp. 10.16: Phase-Sensitive HMBC with BIRD Filter
Exp. 10.17: The Basic HSQC Experime
Exp. 10.18: The HOHAHA or TOCSY Experiment
Exp. 10.19: The NOESY Experiment
Exp. 10.20: The CAMELSPIN or ROESY Experiment
Exp. 10.21: The HOESY Experiment
Exp. 10.22: 2D-INADEQUATE
Exp. 10.23: The EXSY Experiment
Exp. 10.24: X,Y Correlation
· Chapter 11 1D NMR Spectroscopy with Field Gradients
Exp. 11.1: Calibration of Pulsed Field Gradients
Exp. 11.2: Gradient Preemphasis
Exp. 11.3: Gradient Amplifier Test
Exp. 11.4: Determination of Pulsed Field Gradient Ring-Down Delays
Exp. 11.5: The Pulsed Gradient Spin-Echo Experiment
Exp. 11.6: Excitation Pattern of Selective Pulses
Exp. 11.7: The Gradient zz-Filter
Exp. 11.8: gs-SELCOSY
Exp. 11.9: gs-SELTOCSY
Exp. 11.10: DPFGSE-NOE
Exp. 11.11: gs-SELINCOR
Exp. 11.12: GRECCO
Exp. 11.13: WATERGATE
Exp. 11.14: Water Supression by Excitation Sculpting

Chapter 12 2D NMR Spectroscopy with Field Gradients
Exp. 12.1: gs-COSY
Exp. 12.2: Phase-Sensitive gs-DQF-COSY
Exp. 12.3: gs-HMQC
Exp. 12.4: gs-HMBC
Exp. 12.5: ACCORD-HMBC
Exp. 12.6: Phase-Sensititive gs-HSQC with Sensitivity Enhancement
Exp. 12.7: gs-TOCSY
Exp. 12.8: gs-HMQC-TOCSY
Exp. 12.9: 2Q-HMBC
Exp. 12.10: 1H-Detected 2D INEPT-INADEQUATE
Exp. 12.11: gs-NOESY
Exp. 12.12: gs-HSQC-NOESY
Exp. 12.13: gs-HOESY
Exp. 12.14: 1H,15N Correlation with gs-HMQC
· Chapter 13 The Third Dimension
Exp. 13.1: 3D HMQC-COSY
Exp. 13.2: 3D gs-HSQC-TOCSY
Exp. 13.3: 3D H,C,P-Correlation
Exp. 13.4: 3D HMBC
· Chapter 14 Solid-State NMR Spectroscopy
Exp. 14.1: Shimming Solid-State Probe-Heads
Exp. 14.2: Adjusting the Magic Angle
Exp. 14.3: Hartmann-Hahn Matching
Exp. 14.4: The Basic CP/MAS Experiment
Exp. 14.5: TOSS
Exp. 14.6: SELTICS
Exp. 14.7: Multiplicity Determination in the Solid-State

真是开眼界了！

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下面是150 and More Basic NMR Experiments的PDF版,对所列实验的名称,脉冲序列,实验参数有简单的介绍,可供实验者参考.
可以有下面地址下载http://www.rockefeller.edu/nmr/manuals/150_and_more_v2.pdf
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哇塞！！这么多！

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