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【原创】a question about agglomeration of nano particles

  • kgarnett11
    2008/12/18
  • 私聊

透射电镜(TEM)

  • Hi,
    I am a new user. with little experience in TEM.
    I have two questions.
    a), my samples are nano particles, they are pretty easy to agglomerate together. I use ultrasonic to seperate them. but does not work after drying. how you guys do? do you have any tricks to keep them seperate?
    b), how to find the nano particles if they are not uniformaly distributed on the copper grid? say, most of the particles are agglomerated, and some seperated particles at somewhere else but pretty far away from the agglomerated ones, if there is any.
    Thanks very much for your help.
    +关注 私聊
  • earthli

    第1楼2008/12/28

    理解你的意思,
    先用光学显微镜去看看,大概在什么地方。如果不行,你也
    可以在透射电镜也可以到很低的倍数下去找你的样品。
    比如X200左右,

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  • rankin

    第2楼2009/01/01

    也有可能是你的超声时间不够,或者超声的功率不够大
    不过做nano就是这样了,很大一部分时间是要花在找样品上面的

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