Pulse Program Library for Bruker Avance Spectrometers 可进入下面网页在线阅读,粘贴下载。 http://www.nmrfam.wisc.edu/~abild/Pulseprograms/index.html
About this NMR pulse program library
The main emphasis of this pulse program library is directed towards protein NMR spectroscopy of isotope enriched proteins in solution.
All pulse programs are written for the use on Bruker Avance consoles running Xwin-NMR version 2.x. Most sequences will work with Xwin-NMR version 1.3 as well. The rf-channel assignments used are: 1H on f1, 15N on f2, 13C on f3. This may be changed by simply changing the define statement at the top of the pulse program. 例子: 2D 15N-FHSQC, with optional 13C decoupling and SEDUCE-1 decoupling
2D 15N-1H Fast HSQC with minimal water saturation. Use optional 13C decoupling and SEDUCE-1 decoupling with 13C labeled samples. This version uses the gp style gradients.
References Mori et al., J. Magn. Reson. B 108, 94-98 (1995)
Sklenar, Piotto, Leppik, and Saudek: J. Magn. Reson. A 102, 241-245 (1993)
Acquisition Pulse program fhsqc.fa
Include files etc. Include file for optional expt time correction: faexptcorr.incl
Composite pulse decoupling program for SEDUCE-1 decoupling: waltz16sp3
Shaped pulse file for optional compensated SEDUCE-1 decoupling: seduce1c6.jc (JCAMP-DX), seduce1c6.rf (binary RF format) or seduce1c6.txt (ASCII) (cosine modulated SEDUCE-1 shape with excitation optimum at 6*(1/P90) Hz from carrier)
Shaped pulse file for optional compensated SEDUCE-1 decoupling: seduce1c5.jc (JCAMP-DX), seduce1c5.rf (binary RF format) or seduce1c5.txt (ASCII) (cosine modulated SEDUCE-1 shape with excitation optimum at 5*(1/P90) Hz from carrier)
Table of contents About this pulse program library
How to use the files from this library
Legend
T : TROSY C : CryoProbe ready
2D Heteronuclear Shift Correlation fhsqc.fa n15hsqcse.fa cthsqcse.fa c12cosyc12.fa trosy.fa T C trosysefb.fa T C c13cttrosy.fa T
3D/4D Heteronuclear Shift Correlation hncatrkay.fa T hncotrk2b.fa T C hncacbtr.fa T hncocacbtr.fa T hncacotrb.fa T C hncocatr.fa T n15tochsqcse.fa n15tocfhsqc.fa C toccthsqcse.fa hncof.fa C hncose.fa hncaf.fa hncocaf.fa C hncacbf.fa hcchtocsy.fa hcchcosy.fa hcconhse.fa C cconhse.fa C hncacof.fa hncocacbf.fa C hcacose.fa hbacbanhf.fa hbcbconhf.fa cbcaconhse.fa toccthsqcse.fa cdcancocaha.fa C
2D/3D/4D Homonuclear Exchange Spectroscopy - Isotope Enhanced noetrosysefb.fa T noetrosyfb.fa T n15noefhsqc.fa C c13noehsqc.fa c13noe3d.fa cnnoesy4d.fa ccnoesy4d.fa noehncof.fa noecthsqcse.fa hcchnoesy.fa
Relaxation Time Measurement n15t1.fa n15t2.fa hn15noegp.fa hn15noe.fa