定性求助以及其它

应助达人

能否存在网盘或QQ上传，从仪器网下载太难。

是啊，论坛还在抽，我打开帖子都要刷半天，已经上传网盘了，链接是

http://pan.baidu.com/share/link?shareid=171181&uk=1543870179

http://pan.baidu.com/share/link?shareid=171182&uk=1543870179

应助达人

30.496可能和Hedione有关。

感谢朱老师，加仑子醇那个还麻烦朱老师帮看一下

自己顶一下！

自己顶上。。。。。。。。。

应助达人

CASSIFIX（1-Methyl-4-(1,2,2-trimethylbicyclo[3,1,0]hex-3-yl)-2-oxabicyclo[2,2,2]octane）是沸点范围较宽的原料，或者讲不是一个单峰，相关的资料较少，许多是unpublished。

应助达人

A study was conducted to determine some physico-chemical properties of the test material. The freezing point was less than -25 C according to EEC Method A1. The boiling point/boiling range was 301.5 to 309.5 C at 1010 mbar according to EEC Method A2. The relative density (D420) was 0.98591 according to EEC Method A3. The vapour pressure was 1.5 Pa at 25 C according to EEC Method A4. The surface tension was 54.7 mN/m for a 90% saturated aqueous solution at 19.5 C according to EEC Method A5. The water solubility was 1.1 x 10(-2) g/l at 20 C according to EEC Method A6. The partition coefficient was Log P >3.66 at 21 C according to EEC Method A8. The flash point was 144.5 C according to EEC Method A9. The flammability (in contact with water ) was not flammable under the test conditions according to EEC Method A12. The pyrophoric properties of liquids and solids according to EEC Method A13 = not pyrophoric under test conditions. The explosive properties according to EEC Method A14 = no explosive under test conditions. Autoignition temperature (liquids and gases) was 240 C according to EEC Method A15.

应助达人

SPECIFICATIONS
APPEARANCE AT 20°C CLEAR MOBILE LIQUID
COLOR COLORLESS TO PALE YELLOW
ODOR FRESH, HERBAL, FRUITY, CASSIS
TASTE
DENSITY AT 20°C (g/ml) 0,980 - 0,988
REFRACTIVE INDEX nD20 1,4990 - 1,5040
OPTICAL ROTATION (°) 0 / 0
FLASHPOINT (°C) 101
SOLUBILITY SOLUBILITY IN WATER: NON DETERMINED
ASSAY (% GC) PEAK 1+2:20-35;PEAK 3:20-38;PEAK 4:5-16;SUM SEC>98
ACID VALUE (mg KOH/g) -