日本产小松菜检测出恶唑磷、吡螨胺超标。

可惜是日文，一句都看不懂。

ACCESSION: JP010746RECORD_TITLE: ISOXATHION; EI-B; MSDATE: 2011.05.06 (Created 2008.10.21)AUTHORS: HASHIMOTO K, KYOTO COLLEGE OF PHARMACYLICENSE: CC BY-NC-SA

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CH$NAME: ISOXATHIONCH$NAME: O,O-DIETHYL O-5-PHENYLISOXAZOL-3-YL PHOSPHOROTHIOATECH$COMPOUND_CLASS: N/ACH$FORMULA: C13H16NO4PSCH$EXACT_MASS: 313.05377CH$SMILES: CCOP(=S)(OCC)Oc(n2)cc(o2)c(c1)cccc1CH$IUPAC: InChI=1S/C13H16NO4PS/c1-3-15-19(20,16-4-2)18-13-10-12(17-14-13)11-8-6-5-7-9-11/h5-10H,3-4H2,1-2H3

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AC$INSTRUMENT: HITACHI M-80AC$INSTRUMENT_TYPE: EI-BAC$MASS_SPECTROMETRY: MS_TYPE MSAC$MASS_SPECTROMETRY: ION_MODE POSITIVEAC$MASS_SPECTROMETRY: IONIZATION_ENERGY 20 eV

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MS$FOCUSED_ION: ION_TYPE [M]+*

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PK$NUM_PEAK: 66PK$PEAK: m/z int. rel.int.29 2.03 2045 3.05 3161 2.65 2765 3 3077 12.24 12278 1.69 1781 3.24 3289 1.31 1391 1.53 1593 4.17 4297 9.02 9099 1.55 16102 1.29 13103 1.02 10104 1.08 11105 99.99 999106 7.69 77109 10.61 106113 6.16 62114 1.39 14115 1.5 15116 6.46 65121 2.71 27125 5.42 54127 2.21 22128 1.52 15129 2.85 29130 16.12 161131 2.29 23137 1.12 11138 1.01 10141 8.18 82143 1.3 13144 1.02 10145 3.15 32146 1.25 13147 1.27 13149 3.19 32153 1.84 18159 20.36 204160 2.66 27161 9.74 97162 6.35 64169 4.78 48170 1.83 18172 2.95 30174 2.24 22176 1.03 10177 83.25 833178 9.75 98179 4.07 41180 1.13 11186 1.5 15188 1.38 14192 1.52 15205 1.43 14208 9.6 96209 1.12 11239 1.7 17240 1.9 19257 1.44 14285 4.08 41312 1.11 11313 50.77 508314 8.49 85315 3.41 34//

Studies on Persistence of Isoxathion. I. Residue Determination of Isoxathion and Its Oxygen Analog and Preliminary Studies on Persistence of Isoxathion in Crops and Soils

Application of qNMR:Quality control of organophosphorus pesticides

A new method for pesticides identification: fast gc/time-of-flight mass spectrometry

注：暂时搜索完毕。

Liquid chromatography–electrospray quadrupole ion-trap mass spectrometry of nine pesticides in fruits



acrinathrin, carbosulfan, cyproconazole, -cyhalothrin, kresoxim methyl, pyrifenox, pyriproxyfen, propanil, and tebufenpyrad

氟丙菊酯，丁硫克百威，环丙唑醇，三氟氯氰菊酯，醚菌酯，啶斑肟，吡丙醚，敌稗，吡螨胺