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【求助】DSC测试时仪器不能运行

热分析仪

  • 型号为DSC Q10。使用中出现datafile acceptor is not answering的错误提示，但是运行没有什么问题。
    另外仪器无法升温到150度以上，超过150度时自动停止，出现flange temperature limit exceeded的错误信息。但是之前
    做相同试验的时候一切正常，没有问题。
    测试软件为4.9.1版，但是仪器内部软件没有升过，还是原来的购买时的版本。电脑系统为XP SP2

    以下为程序LOG文件
    1 26-Aug-2008 10:22:38 D:\DSC\9309\08-08-24-9309.001
    2 26-Aug-2008 10:22:38 Run 1 completed and saved.
    3 26-Aug-2008 10:12:58 Datafile acceptor is not answering. (681)
    4 26-Aug-2008 10:12:26 Run 1 started.
    5 26-Aug-2008 10:12:23 Air cool turned off. (837)
    6 26-Aug-2008 10:09:46 New day.
    7 24-Aug-2008 11:30:04 Instrument rebooted.
    8 24-Aug-2008 11:29:55 auto_diag_init_at_boot
    9 24-Aug-2008 11:07:27 Datafile not accepted by end of run. Sequence halted. (678)
    10 24-Aug-2008 11:07:27 Flange overtemperature. Run terminated. (067)
    11 24-Aug-2008 11:05:37 Datafile acceptor is not answering. (681)
    12 24-Aug-2008 11:05:03 Run 1 started.
    13 24-Aug-2008 11:05:00 Air cool turned off. (837)
    14 24-Aug-2008 10:52:19 D:\DSC\9306\08-08-23-9306.001
    15 24-Aug-2008 10:52:19 Run 1 completed and saved.
    16 24-Aug-2008 10:43:24 Run 1 started.
    17 24-Aug-2008 10:43:21 Air cool turned off. (837)
    18 24-Aug-2008 10:00:49 D:\DSC\9307\08-08-23-9307.001
    19 24-Aug-2008 10:00:49 Run 1 completed and saved.
    20 24-Aug-2008 09:50:40 Run 1 started.
    21 24-Aug-2008 09:50:37 Air cool turned off. (837)
    22 24-Aug-2008 09:49:57 New day.
    23 23-Aug-2008 15:54:38 Instrument rebooted.
    24 23-Aug-2008 15:54:29 auto_diag_init_at_boot
    25 23-Aug-2008 15:39:44 D:\DSC\fu-bin\08-08-23-FW-103.003
    26 23-Aug-2008 15:39:44 Run 1 completed and saved.
    27 23-Aug-2008 15:39:42 Flange overtemperature. Run terminated. (067)
    28 23-Aug-2008 15:38:37 Run 1 started.
    29 23-Aug-2008 15:38:34 Air cool turned off. (837)
    30 23-Aug-2008 15:38:02 File sent to instrument: C:\FONT\SYSTem08.fnt. (910)
    31 23-Aug-2008 15:37:59 File sent to instrument: C:\FONT\SYSTem01.fnt. (910)
    32 23-Aug-2008 15:37:56 File sent to instrument: C:\FONT\SYSTem00.fnt. (910)
    33 23-Aug-2008 15:37:53 File sent to instrument: C:\FONT\ROMAntri.fnt. (910)
    34 23-Aug-2008 15:37:50 File sent to instrument: C:\FONT\ROMAnsim.fnt. (910)
    35 23-Aug-2008 15:37:47 File sent to instrument: C:\FONT\NEWYrk60.fnt. (910)
    36 23-Aug-2008 15:37:42 File sent to instrument: C:\FONT\LINEs.fnt. (910)
    37 23-Aug-2008 15:37:38 File sent to instrument: C:\FONT\6X10.fnt. (910)
    38 23-Aug-2008 15:37:35 File sent to instrument: C:\TINYLOGO.pcx. (910)
    39 23-Aug-2008 15:26:46 Flange temperature limit exceeded. Cannot start run. (683)
    40 23-Aug-2008 15:26:09 D:\DSC\fu-bin\08-08-23-FW-103.002
    41 23-Aug-2008 15:26:09 Run 1 completed and saved.
    42 23-Aug-2008 15:26:06 Flange overtemperature. Run terminated. (067)
    43 23-Aug-2008 15:24:11 Run 1 started.
    44 23-Aug-2008 15:24:08 Air cool turned off. (837)
    45 23-Aug-2008 15:12:35 Flange temperature limit exceeded. Cannot start run. (683)
    46 23-Aug-2008 15:10:42 Flange temperature limit exceeded. Cannot start run. (683)
    47 23-Aug-2008 15:10:40 Flange temperature limit exceeded. Cannot start run. (683)
    48 23-Aug-2008 15:10:24 D:\DSC\fu-bin\08-08-23-FW-103.001
    49 23-Aug-2008 15:10:24 Run 1 completed and saved.
    50 23-Aug-2008 15:10:19 Flange overtemperature. Run terminated. (067)
    51 23-Aug-2008 15:08:59 Run 1 started.
    52 23-Aug-2008 15:08:56 Air cool turned off. (837)
    53 23-Aug-2008 15:03:51 Instrument rebooted.
    54 23-Aug-2008 15:02:27 Flange temperature limit exceeded. Cannot start run. (7-Aug-23-Aug-2008

    15:03:42 MW auto_diag_init_at_boot
    55 23-Aug-2008 15:01:23 Flange temperature limit exceeded. Cannot start run. (683)
    56 23Aug-2008 15:00:33 Flange temperature limit exceeded. Cannot start run. (683)
    57 23-Aug-2008 15:00:11 Flange temperature limit exceeded. Cannot start run. (683)
    58 23-Aug-2008 14:59:07 Flange temperature limit exceeded. Cannot start run. (683)
    59 23-Aug-2008 14:58:29 Flange temperature limit exceeded. Cannot start run. (683)
    60 23-Aug-2008 14:58:04 Flange temperature limit exceeded. Cannot start run. (683)
    61 23-Aug-2008 14:57:26 Flange temperature limit exceeded. Cannot start run. (683)
    62 23-Aug-2008 14:57:13 Flange temperature limit exceeded. Cannot start run. (683)
    63 23-Aug-2008 14:57:08 Flange temperature limit exceeded. Cannot start run. (683)
    64 23-Aug-2008 14:56:46 Flange temperature limit exceeded. Cannot start run. (683)
    65 23-Aug-2008 14:56:36 Flange temperature limit exceeded. Cannot start run. (683)
    66 23-Aug-2008 14:56:30 Datafile not accepted by end of run. Sequence halted. (678)
    67 23-Aug-2008 14:56:26 Flange overtemperature. Run terminated. (067)
相关话题
    +关注 私聊

  • huan0714

    第1楼2008/08/25

    把异常的过程详细的描述，最好能附上截图或测试的LOG FILE，告知仪器厂家，这样得到的解决方案会更准确~~~

0
    +关注 私聊

  • dnangelhj

    第2楼2008/08/26

    查看一下“Instrument log”，找到错误编号
    然后到帮助里输入错误编号，里面会告诉你原因

0
    +关注 私聊

  • qyw911

    第3楼2008/08/26

    已附上LOG文件，请教

0
    +关注 私聊

  • huan0714

    第4楼2008/08/26

    仪器是用压缩空气制冷的吗？
    测试的升温速率是多少？是不是设定了过温保护而没有打开制冷系统？
    我对TA的仪器不怎么熟，建议最好还是直接问厂家，他们的技术支持还是很不错的。

0
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