好久没有来荧光版面了,作原子荧光多年,去年写了篇英语论文,投了几个国外SCI杂志,拒了几次,还在投稿中。 对其中两条审稿意见,审稿人对涉及原子荧光中前处理试剂的使用的安全性提出质疑。 其一:硝酸-高氯酸消解现在好像还是使用比较多,虽然也有微波消解法,但是微波法虽然时间快,但存在赶酸问题,还有取样量。审稿人建议采用王水法。国际标准就是采用这个消解方法。贴出审稿人意见: It is strongly felt that the routine use of perchloric acid in routine environmental analysis laboratories should not be encouraged on health and safety grounds. Aqua regia digestion is recommended by CEN and ISO standards and is very widely employed