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netzsch 404c DSC 测量5083 h22铝合金的recovery 和recrystallisation的热效应

  • guowei0358
    2011/11/14
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热分析仪

  • 用netzsch 404c DSC 测量5083 h22铝合金的recovery 和recrystallisation的热效应
    样品以annealed 5083作为参考,经过 两个run(不打开chamber)




    有几个小问题:
    1.为什么第一个run在第二个run的下面(出了有明显热效应的部分)
    2.after substraction 之后,基线怎么不在0的位置(似乎和第一问题重合),呵呵
    3.recovery 和recrystallisation的热效应一般是多大啊,在实验中怎么这么不明显
    谢谢大家的赐教,对这个东西实在是理解不了,谢谢
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  • KK-yiqi

    第1楼2011/11/15

    应助达人

    From Wikipedia, the free encyclopedia
    Recrystallization is a process by which deformed grains are replaced by a new set of undeformed grains that nucleate and grow until the original grains have been entirely consumed. Recrystallization is usually accompanied by a reduction in the strength and hardness of a material and a simultaneous increase in the ductility. Thus, the process may be introduced as a deliberate step in metals processing or may be an undesirable byproduct of another processing step. The most important industrial uses are the softening of metals previously hardened by cold work, which have lost their ductility, and the control of the grain structure in the final product.
    Recovery is a process by which deformed grains can reduce their stored energy by the removal or rearrangement of defects in their crystal structure. These defects, primarily dislocations, are introduced by plastic deformation of the material and act to increase the yield strength of a material. Since recovery reduces the dislocation density the process is normally accompanied by a reduction in a materials strength and a simultaneous increase in the ductility. As a result recovery may be considered beneficial or detrimental depending on the circumstances. Recovery is related to the similar process of recrystallisation and grain growth. Recovery competes with recrystallisation, as both are driven by the stored energy, but is also thought to be a necessary prerequisite for the nucleation of recrystallised grains.

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  • guowei0358

    第2楼2011/11/15

    谢谢,但是没有明白这和我问的问题之间的联系。

    KK-yiqi(zhengkang) 发表:From Wikipedia, the free encyclopedia
    Recrystallization is a process by which deformed grains are replaced by a new set of undeformed grains that nucleate and grow until the original grains have been entirely consumed. Recrystallization is usually accompanied by a reduction in the strength and hardness of a material and a simultaneous increase in the ductility. Thus, the process may be introduced as a deliberate step in metals processing or may be an undesirable byproduct of another processing step. The most important industrial uses are the softening of metals previously hardened by cold work, which have lost their ductility, and the control of the grain structure in the final product.
    Recovery is a process by which deformed grains can reduce their stored energy by the removal or rearrangement of defects in their crystal structure. These defects, primarily dislocations, are introduced by plastic deformation of the material and act to increase the yield strength of a material. Since recovery reduces the dislocation density the process is normally accompanied by a reduction in a materials strength and a simultaneous increase in the ductility. As a result recovery may be considered beneficial or detrimental depending on the circumstances. Recovery is related to the similar process of recrystallisation and grain growth. Recovery competes with recrystallisation, as both are driven by the stored energy, but is also thought to be a necessary prerequisite for the nucleation of recrystallised grains.

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  • KK-yiqi

    第3楼2011/11/15

    应助达人

    呵呵,先科普一下.没做过这种材料,这两种热效应有多大,还需查文献后才能补上.有一点不太明白,为何用anneled的作参比,它的性质不会随热历史的改变而改变吗?还是就是要求这种测试方法?

    guowei0358(guowei0358) 发表:谢谢,但是没有明白这和我问的问题之间的联系。

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  • KK-yiqi

    第4楼2011/11/16

    应助达人

    给你一篇文献参考,希望对你有用。的确热不太大。

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  • guowei0358

    第5楼2011/11/19

    非常感谢,一定认真读

    KK-yiqi(zhengkang) 发表:给你一篇文献参考,希望对你有用。的确热不太大。

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