现做一原料残留溶剂方法验证,以DMF为溶剂,检测异丁醇、甲醇、乙腈、二氯甲烷、环己烷和甲苯。 Vial Temp.: 80℃ Loop Temp.: 100℃ Transfer Line Temp.: 120℃ Vial Equilibration Time: 30 min Presurizing Time: 2.0 min Loop Fill Time: 0.5 min Loop Fill Time: 0.05 min Inject Time: 0.05min Injection Port: 140℃ N2: 2.5mL/min 升温程序初始40℃5min然后10℃/min升温至240℃保持2min