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如何调整F20光路系统拍摄高分辨HAADF像

透射电镜(TEM)

  • 请问各位高手,在F20上该如何合轴、调整光路系统做原子尺度的HAADF像呢?
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  • madaowo

    第1楼2013/03/08

    同样感兴趣的顶一下,个人感觉是不是消像散才是关键啊?
    等大牛支招

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  • xdd1987

    第2楼2013/03/09

    关键是如何调出伦奇图吗?

    madaowo(madaowo) 发表:同样感兴趣的顶一下,个人感觉是不是消像散才是关键啊?

    等大牛支招

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  • 大布口袋

    第3楼2013/03/11

    1. Condensor aperture
    2. Rotation center
    4. PPX & PPY
    3. Rongchigram (condensor astigmatism and focus)
    4. On lattice (fine tune condensor astigmatism and focus)

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  • xdd1987

    第4楼2013/03/11

    这个旋转中心一般是怎么调的啊?是尽可能的让像不抖动吗?还是抬小屏看图像是不是向你垂直的跳动?望高手解答!

    大布口袋(taboo) 发表:1. Condensor aperture
    2. Rotation center
    4. PPX & PPY
    3. Rongchigram (condensor astigmatism and focus)

    4. On lattice (fine tune condensor astigmatism and focus)

0
    +关注 私聊
  • madaowo

    第5楼2013/03/14

    How to see the Ronchigram in crystalline samples. Usually I would apply plasma cleaning before TEM My sample is Al-Cu alloy and precipitates with Cu layers sperated by Al layers would be expected. I usually find it difficult to center the C2 aperture (smallest size) due to lack view of Ronchigram, Can you give some practical tips for this operation.

    Of course HRTEM would also work for the purpose. But the contrast would also depend on defocus value. HAADF-STEM seems much less dependent on defocus and is easier for interpretation.

    Thanks!

    大布口袋(taboo) 发表:1. Condensor aperture
    2. Rotation center
    4. PPX & PPY
    3. Rongchigram (condensor astigmatism and focus)

    4. On lattice (fine tune condensor astigmatism and focus)

0
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