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JY ICP光谱仪使用问题收集

ICP光谱

  • 因将邀请吕工来我单位.本人才接触到这种仪器,我想收集一些大家在测试工作中遇到的问题,想难为一下JY技术支持.自己也想学点东西.关于大家提的问题,我会告诉吕老师的,帮助各位解决问题.
      问题可发到我的邮箱yangbin860@163.com
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  • 第1楼2005/11/15

    帮我问一下清洗雾化室用多少浓度的KOH溶液,说明书上就写两片,太模糊了。

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  • 第2楼2005/11/15

    两片就两片,本来KOH就是片状,玻璃怕碱,浓度低还是好,能洗干净就行.张工说用洗涤剂荡一荡也行

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  • 第3楼2005/11/16

    KNOWN PROBLEMS

    After installation over 5.1: some report formats not working
    If you make an installation using option “You have a PREVIOUS version of ICP v5.1 software on your computer”, and if you get a message “rpt not found” for some reports, this can be due to old list of reports.

    To solve that problem, exit V5.2, then:
    1) Delete all files named Report*.* under C:\Program Files\Jobin Yvon SAS\ICP\DB These files can be following:
    (Sometimes Report_Link.db and Report_Link.px does not exist)
    2) Copy from the CD from \SAV\reports list\ the 3 files reports.db reports.mb and reports.px, to directory C:\Program Files\Jobin Yvon SAS\ICP\DB.

    Error In ICP_Indexes Base Index
    This is not a problem, only a message.
    When using Analyst V5.2, and specially when using a data base coming from V5.1, it may happen that the following message is displayed: « Error In ICP_Indexes Base. Index:… »

    For example:
    You should not worry about this message. This message only indicates that the software found wrong indexes and corrected the problem automatically.
    That wrong index may happen after computer power cut off during operation on data base.
    In case of wrong index, software V5.2 corrects the mistake and the error should not appear any more.

    Wrong display in configuration for Poly in some cases
    For Poly, when going in the "board detection" part, if there are 3 boards MVF, the 3 boards are shown at the entrance, but if you click on the button "Board Detection", only 2 boards are shown.
    When opening this part, you have:

    Then after clicking on the button “Board Detection” one acquisition board disappears:

    That does not mean that there is a problem with one MVF board. It is only a problem of display.

    What to do if default sheath gas is not correct when creating a method

    When creating a new method, if the sheath gaz is equal to 0, this not convenient.
    To avoid this problem the text file icpjy_pl.ini must be modified. This file is under folder C:\Program Files\Jobin Yvon SAS\ICP\Bin\CfgFiles.
    The line to modify is
    GainageDebit_ind=1
    It should be modify by:
    GainageDebit_ind=2
    Open this file with notepad, change the value, and close with saving.
    The default value will be G1.

    XP must be in Classical display mode
    Software is not XP mode compatible. It is necessary to modify the XP options for Display from XP Windows to Classical Windows. Especially in Calibration, the grid is destroyed in XP mode.

    Both side print is not possible
    The both side print is not possible as it was possible with V5.1. The correction of this problem is planed for future version.

    Endplasma must be checked before saving the sequence.
    The operation of checking the endplasma box must be done before a sequence is saved. If you check it after saving the sequence, it will not work, and there is no message. The endplasma function of stopping the plasma only works if the box has been checked before the sequence is saved. This will be corrected in future version.

    Some on line helps are missing
    Some part remains with missing on line helps, or on line helps not completed. This will be corrected in future version.

    Some mistakes of English language remain in the English version.
    Some errors of English remain in some parts of the interface. We apologize for these errors, which will be corrected in future version.

    Sheath stabilization time unit in method is displayed “min” instead of “s”.
    The value to be entered is in seconds.

    Impossible to delete a method just used in “Rapid analysis”.
    If you create a method, then run “Rapid analysis” (with one task using this method), then if you decide to delete this method, it will not be possible. You will need to define a task in “rapid analysis” with another method to be able to delete your method.

    Sample name changed to number.
    When viewing from data base of results, using Table, conc/unit/rsd, 3 dec., then exporting using EXCEL 8.0(XLS), the sample name is sometimes changed to a number.

    No indication of overrange
    There is usually no indication on electronic saturation on the print out and export, but only the indication of “out of calibration”

    Not possible to run with level “User”.
    With version 5.2, it is not possible to work at the level “user”. Only level “administrator” is possible. That concern Windows XP Pro and Windows 2000 Pro. Windows NT 4 pack 6 has not been tested.

    Lost of position when running Image from V5.2 with RS232 electronic.
    When you run “Image” from V5.2, if electronic is “RS232- spectralink”, when you come back into the V5.2, the zero order needs to be searched again.

    No wait time after PM change if the limit is specific to PM.
    When changing filters, slits, etc. a wait time is applied. Usually the limit (in wavelength) for changing PM (photomultiplier) corresponds to limit for changing filters. But you can define a different limit for PM in the instrumental configuration. If the limit for PM change does not correspond with other accessory change, then there is no wait time after PM changing. Usually motor move, small necessary time for positioning is enough to avoid problems. Nevertheless, this rare case can be dangerous. If a wavelength very close to the PM limit is analyzed, the first measurement can be wrong due to end of PM positioning. In case of Gaussian, the fir5st points are nearly zero because PM is not in good position. In such case, to avoid that problem, it is necessary to set a high integration time for the line which is concerned, for example 1 second per point, and use a Gaussian with at least 7 points. If other accessories are changed at the same time, the wait time for filters change for example, is enough to avoid this problem.

    Known bugs under Windows 98
    This system is not recommended, because the management of resources of Windows 98 is not adapted to ICP Analyst V5.2. Following problems are known:

    -Method: printing all content of method can crash the software of give wrong graphics for calibration curves. After a calibration, if you go in method and print the calibration results. The coefficients, intensities, etc. are correct, but the curves do not correspond.
    -During print out of sequence results, from sequence, if any problem of paper, etc. whatever), then software hangs up. After rebooting, all results are lost.
    -Fatal errors with blue screen during run of sequence

    By a general way, if resources decrease during run of sequence, any strange error may happen. In case of Windows 98 system, it is possible to decrease the risk of problems by exiting frequently the software, by avoiding to use multi-tasking, and do not run other software at the same time. But problems as print errors in method will remain anyway, and also errors in sequence as Dll_icp_auto, AUTOMSR.EXE errors, illegal operations, unknown error, etc.


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  • 第4楼2005/11/16

    哪个张工?你是哪里的阿

    yb860525 发表:两片就两片,本来KOH就是片状,玻璃怕碱,浓度低还是好,能洗干净就行.张工说用洗涤剂荡一荡也行

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  • 第5楼2005/11/17

    我也搞不清我的雾化室怎么象长霉了似的,我就习惯性地往硝酸里一扔,结果第二天发现密封圈都泡下来了,我往超声里一放,就和毛笔往水里一放似的,黑龙一般,吓了我一跳.可是那"霉"还是没能洗下来.

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  • 第6楼2005/11/21

    我们俩软件一样吗?你说的结果里没有保存这个图标,如果是方法里的话又没有打印预览这个图标.你那是5.2版吗

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  • 第7楼2005/11/24

    你说的保存不是指那个export吧?

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  • 第8楼2006/02/20

    我把这个贴子重新顶起来,每次做我都会遇到新问题,虽说可以解决,但总觉得也不能每次稀里糊涂做,先说一个关于点火的事情
    我每次如果隔夜开机,第二天开电脑就一定点不着火,有时重开电脑有用,有时就要把仪器电源拉一下才行,我想对仪器伤害太大了吧.
    还有护套气我每次选G1,上次做流量计就是显示为0,最后先调到G2,看有反应了再调到G1才好的,就这样做到一半还是Globalrinse了.

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  • 第9楼2006/02/20

    护套气我每次选G1,有时在开机点火前通气发现流量计就是显示为0,(我想是仪器电磁阀出了问题或气路不畅),后来在点火界面调到G2,再通气,就有反应了再调到G1.今天点四五次就是不燃,后来把风机关了,一点就燃(张工以前教的招).搞得我很不爽,以前没这现象,难道是一年不到RF有变.
    仪器软件自己觉得还好,运用了统计过程控制,幸好曾看过"质量工程师"

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  • 第10楼2006/02/20

    老师语:可以用洗液泡,但不要把有密封圈的部分放进去.

    creek 发表:我也搞不清我的雾化室怎么象长霉了似的,我就习惯性地往硝酸里一扔,结果第二天发现密封圈都泡下来了,我往超声里一放,就和毛笔往水里一放似的,黑龙一般,吓了我一跳.可是那"霉"还是没能洗下来.

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